N-氯甲基邻苯二甲酰亚胺合成路线 （共 64 条）
反应条件
1.1: sodium iodide / acetone / 4 h / 20 °C / Darkness 2.1: diethylzinc / hexane; dichloromethane / 18 h / 20 °C / Inert atmosphere 2.2: 4 h / Inert atmosphere View Scheme
参考文献
Maury, Julien; Mouysset, Dominique; Feray, Laurence; Marque, Sylvain R. A.; Siri, Didier; Bertrand, Michele P.
Chemistry - A European Journal, 2012 , vol. 18, # 11 p. 3241 - 3247
反应条件
phosphorous acid trisdiethylamide in acetonitrile T=70 - 80°C;
参考文献
Ivanov, B. E.; Krokhina, S. S.; Chichkanova, T. V.; Kosacheva, E. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 1 p. 162 - 167
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 1 p. 173 - 178
反应条件
1: 76 percent / cesium fluoride, 18-crown-6 / 20 h / Ambient temperature 2: cesium fluoride / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Makio, K.; Yoshioka, H.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 677 - 684
反应条件
18-crown-6 ether; cesium fluoride 20 h; Ambient temperature;
参考文献
Makio, K.; Yoshioka, H.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 677 - 684
反应条件
in Petroleum ether T=90 - 100°C; 2.5 h;
参考文献
Ivanov, B. E.; Krokhina, S. S.; Chichkanova, T. V.; Kosacheva, E. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 1 p. 162 - 167
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 1 p. 173 - 178
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 72 h;
参考文献
D'Ascenzio, Melissa; Carradori, Simone; De Monte, Celeste; Secci, Daniela; Ceruso, Mariangela; Supuran, Claudiu T.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 6 p. 1821 - 1831
反应条件
1,4-dioxane; methanol Herstellung von <1-13C>Glycin beim Kochen des Reaktionsprodukts mit wss.HCl und Essigsaeure;
参考文献
Sakami; Evans; Gurin
Journal of the American Chemical Society, 1947 , vol. 69, p. 1111
反应条件
zinc(II) chloride; benzene
T=70 - 80°C;
参考文献
I.G.Farbenind.
Patent: DE442774 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 15, p. 1701
反应条件
aluminium trichloride in nitromethane
T=48°C; Friedel-Crafts reaction; 0.104722 h; microwave irradiation;
参考文献
Bratulescu; Le Bigot; Delmas
Synthetic Communications, 2001 , vol. 31, # 21 p. 3309 - 3313
参考文献
Teramura et al.
Bl.Inst.chem.Res.Kyoto Univ., 1952 , vol. 28, p. 73
