5 5'-二甲基-2,2'-二吡啶合成路线 （共 36 条）
反应条件
tert-butylaminotris(dimethylamino)phosphazene (phosphazene base P1-t-Bu) in methanol-d4; dichloromethane-d2 T=24.84°C; 1.5 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 49, # 94 p. 11077 - 11079
反应条件
tert-butylaminotris(dimethylamino)phosphazene(phosphazene base P1-t-Bu) in methanol-d4; dichloromethane-d2 T=24.84°C; 2 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 49, # 94 p. 11077 - 11079
反应条件
sodium T=110 - 115°C; 24 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 11 p. 2344 - 2348
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2607 - 2611
参考文献
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, , vol. 80, p. 2693 - 2702
参考文献
Journal of the American Chemical Society, , vol. 68, p. 2574,2576
反应条件
potassium dichromate; sulfuric acid cooling;
参考文献
Dalton Transactions, , # 15 p. 2054 - 2060
反应条件
1: With potassium permanganate; sulfuric acid in water T=-5 - 20°C; 3 - 18 h; Heating / refluxIrradiation; 2: With sodium carbonate in water 3: in water pH=2; Acidic aqueous solution; Product distribution / selectivity;
参考文献
JP2005/82511 A, ;
Page/Page column 4-6 ;
反应条件
1: dichloromethane / 0.08 h / 20 °C / |Inert atmosphere 2: tert-butylaminotris(dimethylamino)phosphazene (phosphazene base P1-t-Bu) / dichloromethane-d2; methanol-d4 / 1.5 h / 24.84 °C / |Inert atmosphere 3: dichloromethane-d2; methanol-d4 / 0.02 h / 24.84 °C / |Inert atmosphere View Scheme
参考文献
Sooksawat, Dhassida; Pike, Sarah J.; Slawin, Alexandra M.Z.; Lusby, Paul J.
Chemical Communications, 2013 , vol. 49, # 94 p. 11077 - 11079
反应条件
in methanol-d4; dichloromethane-d2 T=24.84°C; 0.0166667 h; Inert atmosphere;
参考文献
Sooksawat, Dhassida; Pike, Sarah J.; Slawin, Alexandra M.Z.; Lusby, Paul J.
Chemical Communications, 2013 , vol. 49, # 94 p. 11077 - 11079
反应条件
in methanol-d4; dichloromethane-d2 T=24.84°C; 0.0166667 h; Inert atmosphere; Concentration;
参考文献
Chemical Communications, , vol. 49, # 94 p. 11077 - 11079
