8,8-二氟-1,4-二噁螺[4.5]癸烷合成路线 （共 4 条）
反应条件
XtalFluor-M®; triethylamine tris(hydrogen fluoride) in dichloromethane T=20°C; 24 h;
参考文献
Lheureux, Alexandre; Beaulieu, Francis; Bennett, Christopher; Bill, David R.; Clayton, Simon; Laflamme, Franois; Mirmehrabi, Mahmoud; Tadayon, Sam; Tovell, David; Couturier, Michel
Journal of Organic Chemistry, 2010 , vol. 75, # 10 p. 3401 - 3411
反应条件
pyrrolidinodifluorosulfiniumtetrafluoroborate; triethylamine tris(hydrogen fluoride) in dichloromethane T=20°C; 3 h; Inert atmosphere; Reagent/catalyst;
参考文献
Journal of Fluorine Chemistry, , vol. 153, p. 57 - 60
反应条件
hydrogen; methylamine in methanol; ethanol
参考文献
Flohr, Alexander; Jakob-Roetne, Roland; Norcross, Roger D.; Riemer, Claus
Patent: US2003/149036 A1, 2003 ;
反应条件
hydrogenchloride in acetone 1 h; Inert atmosphere;
参考文献
Chen, Jun; Cook, Matthew J.
Organic Letters, 2013 , vol. 15, # 5 p. 1088 - 1091
