2-叔丁基-1,3-苯并噻唑合成路线 （共 41 条）
反应条件
iron(III) chloride in ethanol
参考文献
Batten; Bentley; Boar; Draper; McGhie; Barton
Journal of the Chemical Society. Perkin transactions 1, 1972 , vol. 5, p. 739 - 748
反应条件
1: With copper diacetate; potassium ethylxanthate in N,N-dimethyl-formamide
T=80°C; Ullmann type reaction; 15 h; Inert atmosphere;
2: With hydrogenchloride in water; N,N-dimethyl-formamide
T=20°C; 8 h; Inert atmosphere;
参考文献
Prasad; Sekar
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 10 p. 1659 - 1665
反应条件
tert.-butyl lithium in tetrahydrofuran
T=-78°C; 0.0833333 h;
参考文献
Katritzky, Alan R.; Kuzmierkiewicz, Wojciech; Aurrecoechea, Jose M.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 844 - 849
反应条件
1: in neat (no solvent)
T=50°C; 1 h; Green chemistry;
2: With 1,3,2-benzodithiazole 1,1,3,3-tetraoxide in neat (no solvent)
T=50°C; 24 h; Green chemistry;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
Arkivoc, 2012 , vol. 2012, # 9 p. 262 - 279
反应条件
pyridine; anhydrous iron chloride; sodium peroxodisulphate in dimethyl sulfoxide
T=40°C; 10 h; Inert atmosphere;
参考文献
Wang, Haibo; Wang, Lu; Shang, Jinsai; Li, Xing; Wang, Haoyuan; Gui, Jie; Lei, Aiwen
Chemical Communications, 2012 , vol. 48, # 1 p. 76 - 78
反应条件
Cu(I) 3-methylsalicylate; oxygen in acetic acid
T=80°C;
参考文献
Hyvl, Jakub; Srogl, Jiri
European Journal of Organic Chemistry, 2010 , # 15 p. 2849 - 2851
反应条件
dipotassium peroxodisulfate; silver nitrate in dichloromethane; water
T=20°C; 8 h; Reagent/catalystSolvent;
参考文献
Zhao, Wei-Ming; Chen, Xiao-Lan; Yuan, Jin-Wei; Qu, Ling-Bo; Duan, Li-Kun; Zhao, Yu-Fen
Chemical Communications, 2014 , vol. 50, # 16 p. 2018 - 2020
反应条件
in toluene
T=20°C; 0.25 h;
参考文献
Rudrawar, Santosh; Kondaskar, Atul; Chakraborti, Asit K.
Synthesis, 2005 , # 15 art. no. Z05105SS, p. 2521 - 2526
反应条件
2-iodobenzothiazole in dimethyl sulfoxide
Irradiation (UV/VIS); mercurial and organic compound dissolved in nitrogen purged solvent, irradn. (350-nm Rayonet photoreactor, 35-40°C, 72h);; mixt. poured into water; extn. with benzene; ext. washed (aq. Na2S2O3), dried (Na2SO4) and concd. (vacuum); yield detd. by (1)H NMR;;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
反应条件
in tetrahydrofuran
T=-78°C; 0.0833333 h;
参考文献
Katritzky, Alan R.; Kuzmierkiewicz, Wojciech; Aurrecoechea, Jose M.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 844 - 849
