(R)-(-)-2-甲氧基-2-苯乙醇合成路线 （共 46 条）
反应条件
cerium(IV) triflate T=80°C; 1 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Iranpoor; Shekarriz; Shiriny
Synthetic Communications, 1998 , vol. 28, # 2 p. 347 - 366
反应条件
cerium(IV) triflate T=80°C; 2 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Iranpoor; Shekarriz; Shiriny
Synthetic Communications, 1998 , vol. 28, # 2 p. 347 - 366
反应条件
1: 37 percent / NaOH / H2O / 1 h / 50 °C 2: 72 percent / BH3 / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 8, # 8 p. 1957 - 1968
反应条件
1: 79 percent / organotin phosphate condensates (OPC) / hexane / 5 h / Heating 2: 89 percent / pyridine / 4 h / Ambient temperature 3: 89 percent / H2 / 5percent Pd-C / ethanol / 72 h / Ambient temperature 4: 85 percent / NaI / acetone / 4 h / Heating 5: 93 percent / DBU / CH2Cl2 / 0.5 h / Ambient temperature 6: 76 percent / pyridine / organotin phosphate condensates (OPC) / Heating View Scheme
参考文献
Tetrahedron, , vol. 47, # 36 p. 7625 - 7634
反应条件
1: organotin phosphate condensates (OPC) / 3 h / Heating 2: KIO4, H2SO4 / ethanol / 0.17 h / 40 °C 3: NaBH4 / ethanol / 2 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 47, # 36 p. 7625 - 7634
反应条件
1: 93 percent / DBU / CH2Cl2 / 0.5 h / Ambient temperature 2: 76 percent / pyridine / organotin phosphate condensates (OPC) / Heating View Scheme
参考文献
Tetrahedron, , vol. 47, # 36 p. 7625 - 7634
反应条件
1: 85 percent / NaI / acetone / 4 h / Heating 2: 93 percent / DBU / CH2Cl2 / 0.5 h / Ambient temperature 3: 76 percent / pyridine / organotin phosphate condensates (OPC) / Heating View Scheme
参考文献
Tetrahedron, , vol. 47, # 36 p. 7625 - 7634
反应条件
1: 89 percent / H2 / 5percent Pd-C / ethanol / 72 h / Ambient temperature 2: 85 percent / NaI / acetone / 4 h / Heating 3: 93 percent / DBU / CH2Cl2 / 0.5 h / Ambient temperature 4: 76 percent / pyridine / organotin phosphate condensates (OPC) / Heating View Scheme
参考文献
Tetrahedron, , vol. 47, # 36 p. 7625 - 7634
反应条件
1: 89 percent / pyridine / 4 h / Ambient temperature 2: 89 percent / H2 / 5percent Pd-C / ethanol / 72 h / Ambient temperature 3: 85 percent / NaI / acetone / 4 h / Heating 4: 93 percent / DBU / CH2Cl2 / 0.5 h / Ambient temperature 5: 76 percent / pyridine / organotin phosphate condensates (OPC) / Heating View Scheme
参考文献
Tetrahedron, , vol. 47, # 36 p. 7625 - 7634
反应条件
1: 91 percent / DMAP; Et3N / CH2Cl2 / 2 h / 20 °C 2: 85 percent / t-BuOK / acetonitrile / 12 h / 20 °C 3: 100 percent / TBAF / acetonitrile / 4 h / 20 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 14, # 4 p. 503 - 510
