1: n-butyllithium / tetrahydrofuran
2: N-bromosuccinmide; water / acetone / 1 h / 20 °C
3: 20 °C
4: Pd0(tris(tert-butyl)phosphine)2; caesium carbonate / tetrahydrofuran; water / 60 °C
View Scheme
参考文献
Matsumoto, Kenji; Shindo, Mitsuru
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 642 - 650
1: N-bromosuccinmide; water / acetone / 1 h / 20 °C
2: 20 °C
3: Pd0(tris(tert-butyl)phosphine)2; caesium carbonate / tetrahydrofuran; water / 60 °C
View Scheme
参考文献
Matsumoto, Kenji; Shindo, Mitsuru
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 642 - 650
1: N-bromosuccinmide / dichloromethane / 11 h / 20 °C
2: n-butyllithium / tetrahydrofuran
3: N-bromosuccinmide; water / acetone / 1 h / 20 °C
4: 20 °C
5: Pd0(tris(tert-butyl)phosphine)2; caesium carbonate / tetrahydrofuran; water / 60 °C
View Scheme
参考文献
Matsumoto, Kenji; Shindo, Mitsuru
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 642 - 650
de Fazi
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1916 , vol. <5> 25 I, p. 97
Gazzetta Chimica Italiana, 1916 , vol. 46 I, p. 277
