反应条件
HCl in isopropyl alcohol byproducts: CO; inert gas; Se (0.025 mmol) treated with NaBH4 (0.056 mmol) in i-PrOH, Fe(CO)5 (0.097 mmol) added at room temp., stirred and refluxed for 12 h; filtered, 5percent aq. HCl added, storred overnight, pptd., septd., washed (H2O, MeOH), dried (vac.), dissolved (toluene), chromd. (SiO2, hexane, toluene);
参考文献
Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, , vol. 34, # 10 p. 739 - 749
