(2E,6E)-2,6-双(3-甲氧基亚苄基)环己酮合成路线 （共 5 条）
反应条件
sodium hydroxide in ethanol T=20°C; 4.5 h;
参考文献
Venugopal, Murugapillai; Elango, Shanmugam; Parthiban, Anbanandam; Eni
Tetrahedron Asymmetry, 2004 , vol. 15, # 21 p. 3427 - 3431
反应条件
1: 78 percent / H2 / Raney nickel / acetone / 12 h / 20 °C
2: pyridine; Br2 / CH2Cl2 / -10 - 20 °C
3: 2.83 g / polyphosphoric acid / 6 h / 105 °C
4: 90 percent / BBr3 / CH2Cl2 / -78 - 20 °C
View Scheme
参考文献
Venugopal, Murugapillai; Elango, Shanmugam; Parthiban, Anbanandam; Eni
Tetrahedron Asymmetry, 2004 , vol. 15, # 21 p. 3427 - 3431
反应条件
hydrogen; nickel in acetone
T=20°C; 12 h;
参考文献
Venugopal, Murugapillai; Elango, Shanmugam; Parthiban, Anbanandam; Eni
Tetrahedron Asymmetry, 2004 , vol. 15, # 21 p. 3427 - 3431
反应条件
1: 78 percent / H2 / Raney nickel / acetone / 12 h / 20 °C
2: pyridine; Br2 / CH2Cl2 / -10 - 20 °C
View Scheme
参考文献
Venugopal, Murugapillai; Elango, Shanmugam; Parthiban, Anbanandam; Eni
Tetrahedron Asymmetry, 2004 , vol. 15, # 21 p. 3427 - 3431
反应条件
1: 78 percent / H2 / Raney nickel / acetone / 12 h / 20 °C
2: pyridine; Br2 / CH2Cl2 / -10 - 20 °C
3: 2.83 g / polyphosphoric acid / 6 h / 105 °C
View Scheme
参考文献
Venugopal, Murugapillai; Elango, Shanmugam; Parthiban, Anbanandam; Eni
Tetrahedron Asymmetry, 2004 , vol. 15, # 21 p. 3427 - 3431
