1-氧-4-氮螺[4.5]癸烷合成路线 （共 10 条）
参考文献
Faidallah, Hassan M.; Sharshira; Al-Saadi, Mohammed S.M.
Heterocyclic Communications, 2009 , vol. 15, # 1 p. 43 - 50
反应条件
1,4-diaza-bicyclo[2.2.2]octane; Hg(II) trifluoroacetate; sodium cyanoborohydride in methanol 24 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sassaman, Mark B.
Tetrahedron, 1996 , vol. 52, # 33 p. 10835 - 10840
反应条件
sodium hydroxide in water
参考文献
Nitrokemia Ipartelepek
Patent: US5055125 A1, 1991 ;
反应条件
1: CH2Cl2 / 20 °C 2: 69 percent / Beauveria bassiana ATCC 7159 / Microbiological reaction 3: IR 120 (H(+)-form / acetonitrile View Scheme
参考文献
Braunegg, Gerhart; De Raadt, Anna; Feichtenhofer, Sabine; Griengl, Herfried; Kopper, Irene; Lehmann, Antje; Weber, Hans-Jorg
Angewandte Chemie - International Edition, 1999 , vol. 38, # 18 p. 2763 - 2766
反应条件
potassium hydroxide Reflux;
参考文献
Sadykov, E. Kh.; Stankevich; Lobanova; Klimenko
Russian Journal of Organic Chemistry, 2014 , vol. 50, # 2 p. 219 - 224
Zh. Org. Khim., 2014 , vol. 50, # 2 p. 226 - 231,6
反应条件
sodium tetrahydroborate in ethanol T=0°C; 0.0833333 h; Yield given;
参考文献
Bayer Corporation
Patent: US6353006 B1, 2002 ;
Location in patent: Page column 86 ;
US 6353006 B1
反应条件
polyphosphoric acid 10 h; Reflux;
参考文献
Sadykov, E. Kh.; Stankevich; Lobanova; Klimenko
Russian Journal of Organic Chemistry, 2014 , vol. 50, # 2 p. 219 - 224
Zh. Org. Khim., 2014 , vol. 50, # 2 p. 226 - 231,6
参考文献
Kukharev
Russian Chemical Bulletin, 1997 , vol. 46, # 8 p. 1482 - 1483
参考文献
Kukharev
Russian Chemical Bulletin, 1997 , vol. 46, # 8 p. 1482 - 1483
反应条件
potassium hydroxide
Reflux;
参考文献
Sadykov, E. Kh.; Stankevich; Lobanova; Klimenko
Russian Journal of Organic Chemistry, 2014 , vol. 50, # 2 p. 219 - 224
Zh. Org. Khim., 2014 , vol. 50, # 2 p. 226 - 231,6
