1,4-二硫杂螺[4.5]癸烷合成路线 （共 34 条）
反应条件
Kaolinitic clay in tetrachloromethane 4 h; Heating;
参考文献
Jnaneshwara; Barhate; Sudalai; Deshpande; Wakharkar; Gajare; Shingare; Sukumar
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 5 p. 965 - 968
反应条件
1: 95 percent / H2O / Nafion-H / acetone / 0.5 h 2: 91 percent / Nafion-H / benzene / Heating View Scheme
参考文献
Olah, George A.; Narang, Subhash C.; Meidar, David; Salem, George F.
Synthesis, 1981 , # 4 p. 282 - 283
反应条件
in tetrachloromethane 4 h; Heatingkaolinitic clay;
参考文献
Jnaneshwara; Barhate; Sudalai; Deshpande; Wakharkar; Gajare; Shingare; Sukumar
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 5 p. 965 - 968
反应条件
N-bromosuccinmide in dichloromethane 1 h;
参考文献
Tani, Hiroyuki; Irie, Shunsuke; Masumoto, Kazunori; Ono, Noboru
Heterocycles, 1993 , vol. 36, # 8 p. 1783 - 1789
反应条件
1: 70 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C 2: conc. aq. HCl / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Masower
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 849,850, 854
J. Gen. Chem. USSR (Engl. Transl.), 1949 , vol. 19, p. 835,836, 840
Chem.Abstr., 1950 , p. 3436
反应条件
1: 30 percent / bis<benzyltriethylammonium> dichromate / hexamethylphosphoric acid triamide / 60 - 80 °C 2: 70 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C 3: conc. aq. HCl / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
反应条件
hydrogenchloride in tetrahydrofuran 0.5 h; Ambient temperature; Yield given;
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
反应条件
2,2'-azo-bisisobutyronitrile in neat (no solvent) T=80°C; 1.5 h; Product distribution;
参考文献
Gutierrez, Carlos G.; Stringham, Rex A.; Nitasaka, Tadashi; Glasscock, Karl G.
Journal of Organic Chemistry, 1980 , vol. 45, # 17 p. 3393 - 3395
反应条件
1: in ethanol T=20°C; 2: With water in ethanol T=20°C;
参考文献
Rohman, Md. Rumum; Rajbangshi, Mantu; Laloo, Badaker M.; Sahu, Priti R.; Myrboh, Bekington
Tetrahedron Letters, 2010 , vol. 51, # 21 p. 2862 - 2864
反应条件
N-halosuccinimide in dichloromethane T=20°C; 0.0833333 h;
参考文献
Karimi, Babak; Seradj, Hassan; Maleki, Jafar
Tetrahedron, 2002 , vol. 58, # 22 p. 4513 - 4516
