1,4-二硫杂螺[4.5]癸烷合成路线 （共 34 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; n-butyllithium
1.) ether, 25 deg C, 2.) -78 deg C -> room temperature; Yield given. Multistep reaction;
参考文献
Wilson, Stephen R.; Georgiadis, Gregory M.; Khatri, Hiralal N.; Bartmess, John E.
Journal of the American Chemical Society, 1980 , vol. 102, # 10 p. 3577 - 3583
反应条件
bromine in chloroform
0.833333 h; Ambient temperatureother substituted cyclohexanone ethanediyl S,S-acetals; different ratio of Br2:substrate; Mechanism;
参考文献
Caputo, Romualdo; Ferreri, Caria; Palumbo, Giovanni; Russo, Francesco
Tetrahedron, 1991 , vol. 47, # 24 p. 4187 - 4194
反应条件
(i), (ii) (alkaline hydrolysis); Multistep reaction;
参考文献
Oishi,T. et al.
Tetrahedron Letters, 1972 , p. 1085 - 1088
反应条件
oxygen; naphthalenyl-1-carbonitrile in water; acetonitrile
Irradiation;
参考文献
Pandey, Bipin; Bal, Smita Y.; Khire, Uday R.
Tetrahedron Letters, 1989 , vol. 30, # 30 p. 4007 - 4008
