4-硝基苯酚三氟甲基磺酸酯合成路线 (共 131 条)
反应条件
triethylamine; palladium diacetate in N,N-dimethyl-formamide T=95°C; 18 h; effect of lithium halides and tetrabutyl ammonium halides on cis/trans ratio, and ratio of α- and β-substitution products; var. solvents; other triflates; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 53, # 9 p. 2112 - 2114
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane; [Fe(II)(C5H5)(C5H4PPh2)] in 1,4-dioxane T=80°C; 14 h;
参考文献
Nising, Carl F.; Schmid, Ulrike K.; Nieger, Martin; Braese, Stefan
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6830 - 6833
反应条件
triethylamine; palladium diacetate in N,N-dimethyl-formamide T=95°C; 18 h; effect of lithium halides and tetrabutyl ammonium halides on cis/trans ratio, and ratio of α- and β-substitution products; var. solvents; other triflates; Product distribution;
参考文献
Andersson, Carl-Magnus; Hallberg, Anders
Journal of Organic Chemistry, 1988 , vol. 53, # 9 p. 2112 - 2114
反应条件
triethylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in propan-1-ol Suzuki cross-coupling reaction; 3 h; Heating;
参考文献
Organic Letters, , vol. 4, # 1 p. 107 - 109
反应条件
caesium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=100°C; 1 h;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Parisi, Luca M.
Synthesis, 2004 , # 11 p. 1889 - 1894
反应条件
potassium acetate; palladium diacetate; 2-(dicyclohexylphosphino)-2'-methylbiphenyl in tetrahydrofuran T=40°C; 17 h; Inert atmosphere;
参考文献
Chang, Joyce Wei Wei; Chia, Eugene Yurong; Chai, Christina Li Lin; Seayad, Jayasree
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 11 p. 2289 - 2299
反应条件
N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=70°C; 5 h; in sealed tube;
参考文献
Journal of the American Chemical Society, , vol. 109, # 9 p. 2831 - 2833
反应条件
caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran; water 18 h; Heating;
参考文献
Molander; Ito
Organic letters, 2001 , vol. 3, # 3 p. 393 - 396
反应条件
in acetonitrile 12 h; Heating;
参考文献
Kotsuki; Kobayashi; Suenaga; Nishizawa
Synthesis, 1990 , # 12 p. 1145 - 1147
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=85°C; 5 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 8 p. 2201 - 2208