1: Methyltriphenylphosphonium bromide With n-butyllithium in tetrahydrofuran
T=0°C; 0.0833333 h;
2: 1-phenyl-2-methyl-1-propanone in tetrahydrofuran
T=20°C;
3: With hydrogenchloride in water
参考文献
Bert, Katrien; Noel, Timothy; Kimpe, Wim; Goeman, Jan L.; Van Der Eycken, Johan
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 42 p. 8539 - 8550
1: Methyltriphenylphosphonium bromide With potassium tert-butylate in tetrahydrofuran
T=0°C; 1 h;
2: 4-nitrophenylacetoaldehyde in tetrahydrofuran
Wittig olefination; Further stages.;
参考文献
Sherrill, William M.; Kim, Ryan; Rubin, Michael
Tetrahedron, 2008 , vol. 64, # 37 p. 8610 - 8617
Behnken, Paul E.; Belmont, James A.; Busby, David C.; Delaney, Mark S.; King, Roswell E.; et al.
Journal of the American Chemical Society, 1984 , vol. 106, p. 3011 - 3025
