顺 -1,2-环己二醇合成路线 （共 184 条）
反应条件
T=250 - 300°C; P=20 Torr; Leiten ueber Aluminiumoxyd;
参考文献
Richter; Ruzicka
Chem. PrumyslChem.Abstr., 1958 , vol. 8, p. 116
Chem. PrumyslChem.Abstr., 1959 , p. 5156
反应条件
T=250 - 300°C; P=20 Torr; Leiten ueber Aluminiumoxyd;
参考文献
Fujita; Nomura
Nippon Kagaku Kaishi, 1942 , vol. 63, p. 510
Chem.Abstr., 1947 , p. 3063
参考文献
Fujita; Nomura
Nippon Kagaku Kaishi, 1942 , vol. 63, p. 510
Chem.Abstr., 1947 , p. 3063
反应条件
iridium (III) chloride trihydrate; oxygen; sodium carbonate; triphenylphosphine in 1,3,5-trimethyl-benzene T=169°C; 15 h;
参考文献
Aramoto, Hiroomi; Obora, Yasushi; Ishii, Yasutaka
Journal of Organic Chemistry, 2009 , vol. 74, # 2 p. 628 - 633
反应条件
4 A molecular sieve; triethylamine; (S)-1-methyl-2-[(N-benzyl-N-methylamino)methyl]pyrrolidine in dichloromethane T=-78°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Mazet, Clement; Koehler, Valentin; Pfaltz, Andreas
Angewandte Chemie - International Edition, 2005 , vol. 44, # 31 p. 4888 - 4891
反应条件
(S)-1-methyl-2-[(dihydroisoindol-2-yl)methyl]pyrrolidine in dichloromethane T=-78°C; 24 h;
参考文献
Kuendig, E. Peter; Enriquez Garcia, Alvaro; Lomberget, Thierry; Perez Garcia, Pablo; Romanens, Patrick
Chemical Communications, 2008 , # 30 p. 3519 - 3521
反应条件
(S)-1-methyl-2-[(dihydroisoindol-2-yl)methyl]pyrrolidine in dichloromethane T=-78°C; 24 h; Yields of byproduct given;
参考文献
Oriyama, Takeshi; Imai, Keisuke; Hosoya, Takeshi; Sano, Tomohumi
Tetrahedron Letters, 1998 , vol. 39, # 5-6 p. 397 - 400
反应条件
(5aS,10bR)-5a,10b-dihydro-2-(pentafluorophenyl)-4H,6H-indeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]oxazinium tetrafluoroborate; 3-benzylriboflavin tetraacetate; triethylamine in chloroform T=20°C; 4 h; AirMolecular sieveResolution of racemate; optical yield given as percent eeenantioselective reaction;
参考文献
Iwahana, Soichiro; Iida, Hiroki; Yashima, Eiji
Chemistry - A European Journal, 2011 , vol. 17, # 29 p. 8009 - 8013
反应条件
4 A molecular sieve; (S)-1-methyl-2-[(dihydroisoindol-2-yl)methyl]pyrrolidine in toluene Yields of byproduct given;
参考文献
Oriyama, Takeshi; Imai, Keisuke; Hosoya, Takeshi; Sano, Tomohumi
Tetrahedron Letters, 1998 , vol. 39, # 5-6 p. 397 - 400
反应条件
Dowex 50W x 2 in toluene T=30°C; Etherification; hydration; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 23 p. 8183 - 8187
