顺 -1,2-环己二醇合成路线 (共 184 条)
反应条件
in chloroform-d1
Kinetics; byproducts: HOCH2CH2OH; inder inert atm., at 25°C, for 0.1 h, in NMR tube; monitoring by (1)H NMR;
参考文献
Roy, Chandra D.; Brown, Herbert C.
Journal of Organometallic Chemistry, 2007 , vol. 692, # 4 p. 784 - 790
参考文献
Roy, Chandra D.; Brown, Herbert C.
Monatshefte fur Chemie, 2007 , vol. 138, # 9 p. 879 - 887
反应条件
in chloroform-d1
T=20°C; 20 h; Title compound not separated from byproducts.;
参考文献
Roy, Chandra D.; Brown, Herbert C.
Monatshefte fur Chemie, 2007 , vol. 138, # 9 p. 879 - 887
反应条件
in chloroform-d1
T=20°C; 5.75 h; Title compound not separated from byproducts.;
参考文献
Roy, Chandra D.; Brown, Herbert C.
Monatshefte fur Chemie, 2007 , vol. 138, # 9 p. 879 - 887
反应条件
dihydrogen peroxide; TAPO-5 in water
T=80°C; 24 h; Further byproducts given;
参考文献
Lee, Sang-Ok; Raja, Robert; Harris, Kenneth D. M.; Thomas, John Meurig; Johnson, Brian F. G.; Sankar, Gopinathan
Angewandte Chemie - International Edition, 2003 , vol. 42, # 13 p. 1520 - 1523
反应条件
diacetate of cis-cyclohexanediol-(1.2);
参考文献
Brunel
Annales de Chimie (Cachan, France), 1905 , vol. <8> 6, p. 208
Bulletin de la Societe Chimique de France, 1905 , vol. <3> 33, p. 269
反应条件
[(neocuproine)Pd(OAc)]2(OTf)2; oxygen in water; acetonitrile
T=25°C; 8 h; Reagent/catalyst; Overall yield = 81 percent; Overall yield = 61 mg;
参考文献
Chung, Kevin; Banik, Steven M.; De Crisci, Antonio G.; Pearson, David M.; Blake, Timothy R.; Olsson, Johan V.; Ingram, Andrew J.; Zare, Richard N.; Waymouth, Robert M.
Journal of the American Chemical Society, 2013 , vol. 135, # 20 p. 7593 - 7602
反应条件
boron trifluoride
T=45°C;
参考文献
Price; Mueller
Journal of the American Chemical Society, 1944 , vol. 66, p. 634
反应条件
hydrogen in n-heptane
T=119.84°C; P=51005.1 Torr; 8 h; AutoclaveInert atmosphere; Kinetics; Solvent;
参考文献
Nakagawa, Yoshinao; Mori, Kazuma; Chen, Kaiyou; Amada, Yasushi; Tamura, Masazumi; Tomishige, Keiichi
Applied Catalysis A: General, 2013 , vol. 468, p. 418 - 425
反应条件
rhenium oxide-modified Ir/SiO2 in water
T=219.84°C; P=7500.75 Torr; 1 h; AutoclaveGreen chemistry;
参考文献
Sato, Hiraku; Tamura, Masazumi; Nakagawa, Yoshinao; Tomishige, Keiichi
Chemistry Letters, 2014 , vol. 43, # 3 p. 334 - 336