顺 -1,2-环己二醇合成路线 (共 184 条)
反应条件
dihydrogen peroxide; dmtacn Mn complex immobilized on amorphous SiO2 in acetonitrile T=-0.15°C; Oxidation; 2 h;
参考文献
Angewandte Chemie - International Edition, , vol. 38, # 7 p. 980 - 983
反应条件
hydrogen in n-heptane T=119.84°C; P=51005.1 Torr; 4 h; AutoclaveInert atmosphere;
参考文献
Applied Catalysis A: General, , vol. 468, p. 418 - 425
反应条件
TiCl3(DME)2; copper; zinc in ethylene glycol dimethyl ether T=25°C; 38 h;
参考文献
McMurry, John E.; Rico, Joseph G.
Tetrahedron Letters, 1989 , vol. 30, # 10 p. 1169 - 1172
反应条件
potassium carbonate in methanol T=23°C; 0.25 h;
参考文献
Corey, E.J.; Das, Jagabandhu
Tetrahedron Letters, 1982 , vol. 23, # 41 p. 4217 - 4220
反应条件
(i-PrS)BBr in dichloromethane T=-78°C;
参考文献
Corey, E. J.; Hua, Duy H.; Seitz, Steven P.
Tetrahedron Letters, 1984 , vol. 25, # 1 p. 3 - 6
反应条件
dihydrogen peroxide; TAPO-5 in water T=80°C; 48 h; Further byproducts given;
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 13 p. 1520 - 1523
反应条件
lithium boron tetrafluoride in acetonitrile T=70°C; 8 h;
参考文献
Uenishi, Jun'ichi; Tanaka, Yusuke; Kawai, Nobuyuki
Tetrahedron Letters, 2006 , vol. 47, # 31 p. 5553 - 5555
反应条件
ammonia in methanol T=-25°C; 4 h;
参考文献
Celik, Murat; Alp, Cemalettin; Coskun, Betuel; Gueltekin, M. Serdar; Balci, Metin
Tetrahedron Letters, 2006 , vol. 47, # 22 p. 3659 - 3663
反应条件
samarium diiodide in tetrahydrofuran 1) -78 deg C, 1 h, 2) to 25 deg C, 2 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 32, # 9 p. 1125 - 1128
反应条件
palladium on activated charcoal in methanol T=30°C; 0.166667 h; atmospheric pressure;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 4-5 p. 727 - 739