顺 -1,2-环己二醇合成路线 （共 184 条）
反应条件
D-glucose in water T=33°C; 24 h; Microbiological reaction; optical yield given as percent ee;
参考文献
Monsalve, Leandro N.; Cerrutti, Patricia; Galvagno, Miguel A.; Baldessari, Alicia
Biocatalysis and Biotransformation, 2010 , vol. 28, # 2 p. 137 - 143
反应条件
hydrogenchloride in methanol; water 24 h; Reflux;
参考文献
Beattie, Christopher; North, Michael; Villuendas, Pedro; Young, Carl
Journal of Organic Chemistry, 2013 , vol. 78, # 2 p. 419 - 426
反应条件
sodium hydroxide in water 24 h; Heating;
参考文献
Goosen, Andre; Hoffman, Eric; Taljaard, Benjamin
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 1 p. 41 - 44
反应条件
1: With sodium tetrahydroborate 2: With hydrogen; platinum(IV) oxide
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 9 p. 1109 - 1112
反应条件
hydrogen; palladium on activated charcoal
参考文献
Journal of Organic Chemistry, , vol. 69, # 18 p. 5966 - 5973
反应条件
1: With dimethylsulfide borane complex in tetrahydrofuran T=0 - 20°C; 2: With benzene-1,2-diol; triethylamine in tetrahydrofuran T=0 - 20°C; 3: With oxygen in tetrahydrofuran T=20°C; 12 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 67, # 21 p. 7193 - 7202
反应条件
1: 85 percent / tosyl chloride, pyridine / CH2Cl2 2: 90 percent / sodium hydride / tetrahydrofuran / 1.) 0 deg C, 2.) 23 deg C, 24 hr 3: 100 percent / 1 N hydrochloric acid / tetrahydrofuran / 0.25 h / 23 °C 4: 95 percent / anhydrous potassium carbonate / methanol / 0.25 h / 23 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 23, # 41 p. 4217 - 4220
反应条件
sodium hydroxide in water Heating;
参考文献
Goosen, Andre; Hoffman, Eric; Taljaard, Benjamin
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 1 p. 41 - 44
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in diethyl ether; toluene T=70°C; Yield given;
参考文献
Tetrahedron, , vol. 48, # 8 p. 1531 - 1538
反应条件
hydrogen; CD; Pt/Al2O3 in toluene T=15°C; P=22501.8 Torr; Kinetics;
参考文献
Journal of Catalysis, , vol. 215, # 1 p. 116 - 121
