顺 -1,2-环己二醇合成路线 (共 184 条)
反应条件
1: glacial acetic acid; water / 100 - 110 °C 2: Hydrolysis View Scheme
参考文献
Journal of the American Chemical Society, , vol. 64, p. 2780,2784
反应条件
sodium hydroxide; dihydrogen peroxide
参考文献
Journal of the American Chemical Society, , vol. 89, p. 4217
反应条件
1: With sodium tetrahydroborate in tetrahydrofuran T=0°C; 2: With silica gel in ethyl acetate
参考文献
Tetrahedron, , vol. 65, # 25 p. 4801 - 4807
反应条件
nickel-cobalt-copper catalyst; decalin T=140°C; P=36775.4 - 73550.8 Torr; Hydrogenation;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 483, p. 31,39
反应条件
nickel-cobalt-copper catalyst; decalin T=140°C; P=36775.4 - 73550.8 Torr; Hydrogenation;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 483, p. 31,39
反应条件
sodium hydroxide; Wilkinson's catalyst; dihydrogen peroxide; benzo[1,3,2]dioxaborole 1.) THF, 20 deg C, 13 h, 2.) THF, EtOH, 20 deg C, 2h; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 114, # 17 p. 6671 - 6679
反应条件
1: With iodosylbenzene; L-proline in N,N-dimethyl-formamide T=20°C; 2: With sodium tetrahydroborate in N,N-dimethyl-formamide T=0°C; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 46, # 12 p. 2053 - 2057
反应条件
1: glacial acetic acid; water / 100 - 110 °C 2: Hydrolysis View Scheme
参考文献
Journal of the American Chemical Society, , vol. 64, p. 2780,2784
反应条件
dihydrogen peroxide; sodium hydroxide in tetrahydrofuran; water T=0 - 20°C;
参考文献
Dalton Transactions, , vol. 42, # 3 p. 746 - 752
反应条件
potassium hydroxide in tetrahydrofuran; water 3 h; Reflux;
参考文献
Beattie, Christopher; North, Michael; Villuendas, Pedro; Young, Carl
Journal of Organic Chemistry, 2013 , vol. 78, # 2 p. 419 - 426