顺 -1,2-环己二醇合成路线 （共 184 条）
反应条件
9-borabicyclo[3.3.1]nonane dimer; alkaline hydrogen peroxide 1.) THF, 25 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 110, # 20 p. 6917 - 6918
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Petroleum Chemistry, , vol. 46, # 1 p. 25 - 27
反应条件
1: 87 percent / CuSO4*5H2O / methanol / 10 h / 0 °C 2: NaBH4 / methanol / 0.33 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 18 p. 5966 - 5973
反应条件
CF3O3S(1-)*C20H18F6N4O6OsS2(1+); dihydrogen peroxide in water; tert-butyl alcohol T=30°C; pH=4; Inert atmosphere; Temperature;
参考文献
Sugimoto, Hideki; Kitayama, Kazuhiro; Mori, Seiji; Itoh, Shinobu
Journal of the American Chemical Society, 2012 , vol. 134, # 46 p. 19270 - 19280
反应条件
(S)-3-{6-[(ethyl-phenylamino)-methyl]-pyridin-2-yl}-2-hydroxy-2-phenylpropionic acid; dihydrogen peroxide; ferrous acetate in methanol; water T=20°C; 16 h;
参考文献
Synlett, , # 14 p. 2172 - 2174
反应条件
potassium hydroxide; Raney Ni-Al alloy in water T=90°C; 6 h; optical yield given as percent de;
参考文献
Journal of Chemical Research, , # 6 p. 342 - 344
反应条件
1: 56 percent / Re2O7 2: 80percent CF3CO2H / 0.5 h / 0 °C 3: NaBH4 / methanol View Scheme
参考文献
Tetrahedron Letters, , vol. 33, # 51 p. 7823 - 7826
反应条件
1: 80percent CF3CO2H / 0.5 h / 0 °C 2: NaBH4 / methanol View Scheme
参考文献
Tetrahedron Letters, , vol. 33, # 51 p. 7823 - 7826
反应条件
1: 100 percent / 1 N hydrochloric acid / tetrahydrofuran / 0.25 h / 23 °C 2: 95 percent / anhydrous potassium carbonate / methanol / 0.25 h / 23 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 23, # 41 p. 4217 - 4220
反应条件
1: 90 percent / sodium hydride / tetrahydrofuran / 1.) 0 deg C, 2.) 23 deg C, 24 hr 2: 100 percent / 1 N hydrochloric acid / tetrahydrofuran / 0.25 h / 23 °C 3: 95 percent / anhydrous potassium carbonate / methanol / 0.25 h / 23 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 23, # 41 p. 4217 - 4220
