potassium carbonate in N,N-dimethyl-formamide
T=60 - 70°C; 3 h;
参考文献
Vereshchagin, L. I.; Kirillova, L. P.; Luzgina, G. M.; Gareev, G. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 1 p. 29 - 33
Zhurnal Organicheskoi Khimii, 1984 , vol. l, # 1 p. 34 - 38
1: phenol With sodium hydride in N,N-dimethyl-formamide; mineral oil
T=0 - 23°C; Inert atmosphere;
2: 1-(3-bromo-1-propynyl)benzene in N,N-dimethyl-formamide; mineral oil
T=23°C; 4 h; Inert atmosphere;
1: dihydrogen peroxide; silver nitrate / diethyl ether / 19 h / 0 - 20 °C
2: PPh3 gold(I) chloro complex; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; water / dichloromethane / 20 h / 20 °C
View Scheme
参考文献
Alcaide, Benito; Almendros, Pedro; Quiros, M. Teresa; Lopez, Ramon; Menendez, Maria I.; Sochacka-Cwikla, Aleksandra
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 898 - 905
