反应条件
1: sodium hydride / tetrahydrofuran / 72 h / 0 - 20 °C / Inert atmosphere
2: palladium 10 on activated carbon; perchloric acid; hydrogen / ethanol
3: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
4: triethylamine / 6 h / -78 - 20 °C / UV-irradiation
View Scheme
参考文献
Drouin, Alexandre; Winter, Dana K.; Pichette, Simon; Aubert-Nicol, Samuel; Lessard, Jean; Spino, Claude
Journal of Organic Chemistry, 2011 , vol. 76, # 1 p. 164 - 169