2-三正丁基甲锡烷基吡啶合成路线 （共 97 条）
反应条件
PhCH2Pd(PPh3)2Cl in toluene 12 h; Heating;
参考文献
Sosabowski, Michael H.; Powell, Paul
Journal of Chemical Research, Miniprint, 1997 , # 1 p. 201 - 219
反应条件
aluminium trichloride in dichloromethane T=-78°C; 4 h;
参考文献
Niestroj, Michael; Neumann, Wilhelm P.
Chemische Berichte, 1996 , vol. 129, # 1 p. 45 - 51
反应条件
tris-(dibenzylideneacetone)dipalladium(0); cesium fluoride; tris-(o-tolyl)phosphine; copper(I) bromide in 1-methyl-pyrrolidin-2-one T=60°C; 0.0833333 h; Inert atmosphere;
参考文献
Suzuki, Masaaki; Sumi, Kengo; Koyama, Hiroko; Siqin; Hosoya, Takamitsu; Takashima-Hirano, Misato; Doi, Hisashi
Chemistry - A European Journal, 2009 , vol. 15, # 45 p. 12489 - 12495
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene 11 h; Reflux;
参考文献
Shinonogi and Co., Ltd
Patent: US2011/28468 A1, 2011 ;
Location in patent: Page/Page column 22 ;
反应条件
(Ph3Ph)4Pd in toluene T=110°C; Substitution; Stille coupling; 16 h;
参考文献
Fallahpour, Reza-Ali
Synthesis, 2000 , # 8 p. 1138 - 1142
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(II) oxide in N,N-dimethyl-formamide T=160°C; Stille coupling; 0.25 h; Inert atmosphereMicrowave irradiation;
参考文献
Wang, Zixing; Turner, Eric; Mahoney, Vanessa; Madakuni, Sijesh; Groy, Thomas; Li, Jian
Inorganic Chemistry, 2010 , vol. 49, # 24 p. 11276 - 11286
反应条件
1: lithium chloride; bis-triphenylphosphine-palladium(II) chloride / toluene / 10 h / 110 °C / |Inert atmosphere 2: tris-(dibenzylideneacetone)dipalladium(0); 1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate / toluene / 30 h / 110 °C / |Inert atmosphere View Scheme
参考文献
Tang, Jian-Hong; Wu, Si-Hai; Shao, Jiang-Yang; Nie, Hai-Jing; Zhong, Yu-Wu
Organometallics, 2013 , vol. 32, # 16 p. 4564 - 4570
反应条件
bis-triphenylphosphine-palladium(II) chloride; lithium chloride in toluene T=150°C; 48 h; Inert atmosphere;
参考文献
Yao, Chang-Jiang; Zheng, Ren-Hui; Shi, Qiang; Zhong, Yu-Wu; Yao, Jiannian
Chemical Communications, 2012 , vol. 48, # 45 p. 5680 - 5682
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=100°C;
参考文献
Haino, Takeharu; Araki, Hiromi; Yamanaka, Yuko; Fukazawa, Yoshimasa
Tetrahedron Letters, 2001 , vol. 42, # 18 p. 3203 - 3206
反应条件
tetrakis(triphenylphosphine) palladium(0); silver(l) oxide 1) DMF, 5 min, 100 deg C, 2) DMF, 80-90 min, 100 deg C; Yield given. Multistep reaction;
参考文献
Malm, Johan; Bjoerk, Patrick; Gronowitz, Salo; Hoernfeldt, Anna-Britta
Tetrahedron Letters, 1992 , vol. 33, # 16 p. 2199 - 2202
