N,N-二甲基-2,3,4,5,6-五氟苯胺合成路线 (共 12 条)
反应条件
potassium tert-butylate in tetrahydrofuran
T=20°C; 0.166667 h;
参考文献
Roberts, Kenneth M.; Jones, Jeffery P.
Chemistry - A European Journal, 2010 , vol. 16, # 27 p. 8096 - 8107
反应条件
in methanol
T=100°C; 5 h;
参考文献
Kobayashi,H.; Sonoda,T.
Journal of Fluorine Chemistry, 1985 , vol. 27, p. 1
反应条件
HCOOH, formaline
18 h in reflux with 90percent HCOOH, at heating for only 6 h an unknown byproduct formed;
参考文献
Allen, J. G.; Burdon, J.; Tatlow, J.C.
Journal of the Chemical Society, 1965 , p. 6329 - 6336
参考文献
Blazejewski, Jean-Claude; Wakselman, Claude
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2845 - 2850
反应条件
1: H2O
2: HCOOH, formaline
View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
反应条件
1: HI
2: HCOOH, formaline
View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
参考文献
Allen, J. G.; Burdon, J.; Tatlow, J.C.
Journal of the Chemical Society, 1965 , p. 6329 - 6336
反应条件
T=160°C; 82 h; Product distribution; Further Variations:Temperaturestime;
参考文献
Zhang, Cheng-Pan; Chen, Qing-Yun; Xiao, Ji-Chang
Journal of Fluorine Chemistry, 2008 , vol. 129, # 5 p. 424 - 428