acetic acid 0.5 h; Heating;

acetic acid 0.5 h; Heating;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605283', constants.ctx, '0')">triethylamine</a> <br />T=5 - 10&deg;C;&nbsp;0.166667&nbsp;h;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: PCl₃, Et₃N / toluene / 1.) -78 deg C, 2 h, 2.) -20 deg C, 10 h<br />2: Et₃N / 0.17 h / 5 - 10 &deg;C<br /> <br /> &nbsp;