1,4-二氧代-2,3-二溴甲基喹啉合成路线 （共 10 条）
反应条件
HOF* CH3CN in chloroform T=0°C;
参考文献
Carmeli, Mira; Rozen, Shlomo
Journal of Organic Chemistry, 2006 , vol. 71, # 15 p. 5761 - 5765
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=25°C; 42 h;
参考文献
Pearson, Russell J.; Evans, Kathryn M.; Slawin, Alexandra M. Z.; Philp, Douglas; Westwood, Nicholas J.
Journal of Organic Chemistry, 2005 , vol. 70, # 13 p. 5055 - 5061
反应条件
bromine in ethyl acetate Heating;
参考文献
Haddadin, Makhluf J.; Samaha, Mona S.; Hajj-Ubayd, Antoun B.
Heterocycles, 1992 , vol. 33, # 2 p. 541 - 544
反应条件
1: 88 percent / tetrahydrofuran / 17 h / 20 °C 2: 41 percent / m-chloroperoxybenzoic acid / CH2Cl2 / 20 h / 25 °C View Scheme
参考文献
Pearson, Russell J.; Evans, Kathryn M.; Slawin, Alexandra M. Z.; Philp, Douglas; Westwood, Nicholas J.
Journal of Organic Chemistry, 2005 , vol. 70, # 13 p. 5055 - 5061
反应条件
1: 65 percent / pyrrolidine / acetonitrile / Heating 2: 85 percent / Br2 / ethyl acetate / Heating View Scheme
参考文献
Haddadin, Makhluf J.; Samaha, Mona S.; Hajj-Ubayd, Antoun B.
Heterocycles, 1992 , vol. 33, # 2 p. 541 - 544
反应条件
sodium hydroxide; tetrabutylammomium bromide in chloroform; water T=56°C; 20 h;
参考文献
Fridman, I. A.; Nikonova, I. V.; Koldobskii, G. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1994 , vol. 30, # 6 p. 713 - 717
Khimiya Geterotsiklicheskikh Soedinenii, 1994 , # 6 p. 816 - 820
反应条件
in dimethyl sulfoxide Heating;
参考文献
Haddadin, Makhluf J.; Samaha, Mona S.; Hajj-Ubayd, Antoun B.
Heterocycles, 1992 , vol. 33, # 2 p. 541 - 544
参考文献
Landquist; Silk
Journal of the Chemical Society, 1956 , p. 2052,2055
反应条件
in ethanol 504 h; Irradiation;
参考文献
Dvoryantseva, G. G.; Tetenchuk, K. P.; Pol'shakov, V. I.; Elina, A. S.
Pharmaceutical Chemistry Journal, 1986 , vol. 20, # 4 p. 227 - 235
Khimiko-Farmatsevticheskii Zhurnal, 1986 , vol. 20, # 4 p. 399 - 408
反应条件
2: aqueous HCl View Scheme
参考文献
Landquist; Silk
Journal of the Chemical Society, 1956 , p. 2052,2055
