3,4-双乙酸基-1丁烯合成路线 (共 20 条)
反应条件
acetic acid in dichloromethane T=40°C; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 132, # 43 p. 15185 - 15191
反应条件
palladium diacetate in dichloromethane T=23°C; 2 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 132, # 43 p. 15185 - 15191
反应条件
pyridine in diethyl ether 1.) room temp., 14 h; 2.) reflux, 6 h;
参考文献
Synthesis, , # 6 p. 469 - 471
反应条件
tetrakis(triphenylphosphine) palladium(0) in dichloromethane T=20°C; 48 h;
参考文献
Tetrahedron Letters, , vol. 49, # 41 p. 5843 - 5846
反应条件
triphenylphosphine; platinum (II) chloride T=120 - 160°C; P=76.0051 - 760.051 Torr; 12 - 14.5 h; Heating / reflux; Product distribution / selectivity;
参考文献
US2009/54717 A1, ;
Page/Page column 4-5 ;
反应条件
[(Rp,S)-COP-OAc]2 in dichloromethane T=38°C; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 132, # 43 p. 15185 - 15191
参考文献
Journal of the Chemical Society, , p. 247
反应条件
sodium acetate in acetic anhydride; acetic acid T=60°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 37, p. 291 - 295
反应条件
oxygen; Rh-Ge T=80 - 85°C; P=56254.5 - 60004.8 Torr; 5 h; other catalysts; Product distribution;
参考文献
Russian Journal of Applied Chemistry, , vol. 67, # 2.1 p. 221 - 224
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), , vol. 67, # 2 p. 244 - 248
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=70°C; Product distribution; Further Variations:Solvents;
参考文献
European Journal of Organic Chemistry, , # 17 p. 3301 - 3305