(苯基氧代甲基)膦酸二甲酯合成路线 （共 52 条）
反应条件
in benzene 12 h; Ambient temperature;
参考文献
Breuer, Eli; Karaman, Rafik; Goldblum, Amiram; Leader, Haim
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 2029 - 2034
反应条件
1.) benzene, r.t., 12 h; 2.) benzene, 4 h, reflux; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Breuer, Eli; Karaman, Rafik; Goldblum, Amiram; Leader, Haim
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 2029 - 2034
反应条件
in benzene 24 h; Heatingvariation of time and concentrations; other dialkyl acylphosphonates; Product distributionMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 2029 - 2034
反应条件
hydrazine hydrate in ethanol T=0°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Breuer, Eli; Safadi, Muhammad; Chorev, Michael; Gibson, Dan
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 60, # 3/4 p. 239 - 246
反应条件
potassium carbonate in acetonitrile T=60°C; Darzens type reaction; Inert atmosphere;
参考文献
Demir, Ayhan S.; Emrullahoglu, Mustafa; Pirkin, Eser; Akca, Nazmiye
Journal of Organic Chemistry, 2008 , vol. 73, # 22 p. 8992 - 8997
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran T=25°C; Inert atmosphere;
参考文献
Demir, Ayhan S.; Emrullahoglu, Mustafa; Pirkin, Eser; Akca, Nazmiye
Journal of Organic Chemistry, 2008 , vol. 73, # 22 p. 8992 - 8997
反应条件
in acetonitrile T=25°C; Darzens type reaction; Inert atmosphere;
参考文献
Demir, Ayhan S.; Emrullahoglu, Mustafa; Pirkin, Eser; Akca, Nazmiye
Journal of Organic Chemistry, 2008 , vol. 73, # 22 p. 8992 - 8997
反应条件
in acetonitrile 1.5 h; Ambient temperature;
参考文献
Migianu, Evelyne; Monteil, Maelle; Even, Pascale; Lecouvey, Marc
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 2 p. 121 - 133
反应条件
in tetrachloromethane T=0 - 10°C;
参考文献
Blackburn, G. Michael; Ingleson, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1150 - 1153
反应条件
trimethylsilyl bromide
参考文献
McKenna,C.E. et al.
Tetrahedron Letters, 1977 , # 2 p. 155 - 158
