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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-氯-4-甲氧基苯酚
合成路线
（共 27 条）
150-76-5
4-甲氧基苯酚
→
反应条件
18113-03-6
2-氯-4-甲氧基苯酚
反应条件
N-chloro-3-methyl-2,6-diphenylpiperidin-4-one; hydrogen cation in ethanol; water T=30°C; ΔH(excit.), ΔS(excit.); Product distributionThermodynamic data;
参考文献
Journal of the Indian Chemical Society, , vol. 66, # 5 p. 301 - 303
1131890-97-5
→
反应条件
622-97-9
4-甲基苯乙烯
+
18113-03-6
2-氯-4-甲氧基苯酚
+
1262210-20-7
反应条件
tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butylate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane T=110°C; Heck reaction; 20 h; Inert atmosphereReflux;
参考文献
Organic Letters, , vol. 13, # 3 p. 510 - 513
935-50-2
4,4-二甲氧基-2,5-环己二烯-1-酮
→
反应条件
18113-03-6
2-氯-4-甲氧基苯酚
反应条件
N,N'-dimethylhydrazine bishydrochloride in acetonitrile 0.5 h; Reflux; Reagent/catalyst; regioselective reaction;
参考文献
Yin, Zhiwei; Zhang, Jinzhu; Wu, Jing; Green, Riana; Li, Sihan; Zheng, Shengping
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 18 p. 2854 - 2858
139139-72-3
→
反应条件
18113-03-6
2-氯-4-甲氧基苯酚
反应条件
N,N'-dimethylhydrazine bishydrochloride in acetonitrile 0.5 h; Reflux; regioselective reaction;
参考文献
Yin, Zhiwei; Zhang, Jinzhu; Wu, Jing; Green, Riana; Li, Sihan; Zheng, Shengping
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 18 p. 2854 - 2858
108-95-2
苯酚
→
反应条件
18113-03-6
2-氯-4-甲氧基苯酚
反应条件
1: [bis(acetoxy)iodo]benzene 2: N,N'-dimethylhydrazine bishydrochloride / acetonitrile / 0.5 h / |Reflux View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 18 p. 2854 - 2858
108534-51-6
→
反应条件
18113-03-6
2-氯-4-甲氧基苯酚
反应条件
N,N'-dimethylhydrazine bishydrochloride in acetonitrile 0.5 h; Reflux; regioselective reaction;
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 18 p. 2854 - 2858
108-95-2
苯酚
→
反应条件
18113-03-6
2-氯-4-甲氧基苯酚
+
344326-18-7
2-氯-4-乙氧基苯酚
反应条件
1: [bis(acetoxy)iodo]benzene 2: N,N'-dimethylhydrazine bishydrochloride / acetonitrile / 1 h / |Reflux View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 18 p. 2854 - 2858
64-17-5
乙醇
+
935-50-2
4,4-二甲氧基-2,5-环己二烯-1-酮
→
反应条件
18113-03-6
2-氯-4-甲氧基苯酚
+
344326-18-7
2-氯-4-乙氧基苯酚
反应条件
N,N'-dimethylhydrazine bishydrochloride in acetonitrile 1 h; Reflux; regioselective reaction;
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 18 p. 2854 - 2858
73010-52-3
→
反应条件
18113-03-6
2-氯-4-甲氧基苯酚
+
344326-18-7
2-氯-4-乙氧基苯酚
反应条件
N,N'-dimethylhydrazine bishydrochloride 0.5 h; Reflux; Overall yield = 24 mg; regioselective reaction;
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 18 p. 2854 - 2858
73010-54-5
→
反应条件
860616-67-7
+
18113-03-6
2-氯-4-甲氧基苯酚
反应条件
N,N'-dimethylhydrazine bishydrochloride 0.5 h; Reflux; Overall yield = 65 mg; regioselective reaction;
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 18 p. 2854 - 2858
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