2,5-二氯-2,5-二甲基-2,5-二硅杂-3-己炔合成路线 (共 4 条)
反应条件
chlorine in tetrachloromethane 3 h; Ambient temperature;
参考文献
Wrackmeyer, Bernd; Kehr, Gerald; Suess, Juergen; Molla, Elias
Journal of Organometallic Chemistry, 1998 , vol. 562, # 2 p. 207 - 215
参考文献
Frisch; Young
Journal of the American Chemical Society, 1952 , vol. 74, p. 4853,4855
反应条件
pyridine; thionyl chloride
参考文献
Komarov,N.V. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1963 , p. 86 - 93
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1963 , # 1 p. 97 - 105
反应条件
in hexane reaction at room temp. for 16 h under Ar using Schlenk or glove-box technique;
参考文献
Lamac, Martin; Spannenberg, Anke; Jiao, Haijun; Hansen, Sven; Baumann, Wolfgang; Arndt, Perdita; Rosenthal, Uwe
Angewandte Chemie - International Edition, 2010 , vol. 49, # 16 p. 2937 - 2940