4-苯基-3-丁炔-2-酮合成路线 （共 131 条）
反应条件
1: 85 percent / benzene / 2 h / Ambient temperature 2: 77 percent / 1 h / 210 °C / 0.01 Torr 3: 1.) n-BuLi / 1.) hexane, THF, -78 deg C to room temp., 2.) 4 h, room temp. View Scheme
参考文献
Synthesis, , # 3 p. 240 - 243
反应条件
n-Butyl nitrite in benzene Heating;
参考文献
Bulletin de la Societe Chimique de France, , p. 210 - 217
反应条件
1: 80 percent / diethyl ether / 20 °C 2: 88 percent / aq. HCl / diethyl ether / 2 h / Ambient temperature View Scheme
参考文献
Chemistry of Heterocyclic Compounds, , vol. 32, # 2 p. 169 - 173
参考文献
Journal of the American Chemical Society, , vol. 67, p. 416,417
Journal of the American Chemical Society, , vol. 69, p. 1181,1182
反应条件
aluminium trichloride in carbon disulfide Heating;
参考文献
Chemische Berichte, , vol. 96, p. 3280 - 3288
反应条件
Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 32, # 48 p. 7091 - 7092
反应条件
methyllithium ether; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 55, # 10 p. 3368 - 3370
反应条件
1: 77 percent / 1 h / 210 °C / 0.01 Torr 2: 1.) n-BuLi / 1.) hexane, THF, -78 deg C to room temp., 2.) 4 h, room temp. View Scheme
参考文献
Synthesis, , # 3 p. 240 - 243
反应条件
n-butyllithium; boron trifluoride diethyl etherate 1.) THF, hexane, -78 deg C, 10 min; 2.) -78 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Synthesis, , # 5 p. 421 - 422
反应条件
n-butyllithium; boron trifluoride diethyl etherate 1.) THF, hexane, -78 deg C, 10 min; 2.) -78 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Synthesis, , # 5 p. 421 - 422
