5-溴-2-碘苯甲酸甲酯合成路线 （共 14 条）
反应条件
formic acid; tributyl-amine; tris-fac-Ir(ppy)3 in acetonitrile T=25 - 30°C; 24 h; Inert atmosphereIrradiation;
参考文献
Nature Chemistry, , vol. 4, # 10 p. 854 - 859
反应条件
1.1: diisobutylaluminium hydride / tetrahydrofuran; dichloromethane / 0 - 20 °C / Inert atmosphere 1.2: 0 °C / Inert atmosphere 2.1: dipyridinium dichromate / dichloromethane / 4 h / 20 °C / Inert atmosphere View Scheme
参考文献
Zhou, Ningzhang; Wang, Li; Thompson, David W.; Zhao, Yuming
Tetrahedron, 2011 , vol. 67, # 1 p. 125 - 143
反应条件
1,3-bis-(diphenylphosphino)propane; palladium diacetate; caesium carbonate in toluene
T=95°C; 24 h;
参考文献
Worlikar, Shilpa A.; Larock, Richard C.
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7175 - 7180
反应条件
T=180°C; Erwaermen des Reaktionsprodukts mit Schwefelsaeure;
参考文献
Rule; Smith
Journal of the Chemical Society, 1937 , p. 1096,1101
