4-(1,2-二苯乙烯基)吗啉合成路线 (共 4 条)
反应条件
Li[B(C6F5)4]*2.5(Et2O); [Au(dimethyl sulfide)Cl]; N,N-dimethyl-2-(diphenylphosphino)benzeneaniline in 1,4-dioxane T=110°C; 1 h; Product distribution / selectivity;
参考文献
DALHOUSIE UNIVERSITY; LUNDGREN, Rylan, J.; STRADIOTTO, Mark
Patent: WO2012/68335 A2, 2012 ;
Location in patent: Page/Page column 52-53 ;
反应条件
hydrogenchloride; water in tetrahydrofuran 3 h; Ambient temperature; Yield given;
参考文献
Broekhof, N. L. J. M.; Elburg, P. van; Hoff, D. J.; Gen, A. van der
Recueil: Journal of the Royal Netherlands Chemical Society, 1984 , vol. 103, # 11 p. 317 - 321
反应条件
1-fluoro-2-pyridone in dichloromethane
49 h; Heating;
参考文献
Purrington, Suzanne T.; Jones, Walda Ann
Journal of Fluorine Chemistry, 1984 , vol. 26, p. 43 - 46
反应条件
(i) EtOH, (ii) aq. HCl, MeOH; Multistep reaction;
参考文献
Kuehne,M.E.; Foley,L.
Journal of Organic Chemistry, 1965 , vol. 30, p. 4280 - 4284