2-氨基-6-甲基吡啶合成路线 (共 244 条)
反应条件
copper(I) oxide; potassium carbonate; ammonium hydroxide; N,N-dimethylethylenediamine in ethylene glycol T=60°C; 16 h; Inert atmosphere;
参考文献
Elmkaddem, Mohammed K.; Fischmeister, Cedric; Thomas, Christophe M.; Renaud, Jean-Luc
Chemical Communications, 2010 , vol. 46, # 6 p. 925 - 927
反应条件
ammonium hydroxide; potassium phosphate; 1-(5,6,7,8-tetrahydroquinolin-8-yl)-2-methylpropan-1-one; copper(I) bromide in dimethyl sulfoxide T=25°C; 24 h; Inert atmosphereSealed tube;
参考文献
Wang, Deping; Cai, Qian; Ding, Ke
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 11-12 p. 1722 - 1726
反应条件
ammonia; sodium; toluene T=130°C;
参考文献
DE358397 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 529
反应条件
titanium tetrachloride; tin(ll) chloride in diethyl ether 0.5 h; Ambient temperature;
参考文献
Balicki, Roman; Kaczmarek, Lukasz; Malinowski, Marek
Synthetic Communications, 1989 , vol. 19, # 5and6 p. 897 - 900
反应条件
hydroxylamine hydrochloride in ethanol; water 24 h; Heating;
参考文献
Bruekelman, Stephen P.; Leach, (Miss) Susan E.; Meakins, G. Denis; Tirel, Malcolm D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2801 - 2807
反应条件
sodium hydroxide T=70°C; 1 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 58, # 4 p. 887 - 891
反应条件
hydrogenchloride 3 h; Heating;
参考文献
Wachi, Kazuyuki; Terada, Atsusuke
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 10 p. 3020 - 3028
反应条件
1: CH2Cl2 / Heating 2: conc. HCl View Scheme
参考文献
Bioorganic and medicinal chemistry letters, , vol. 10, # 17 p. 1975 - 1978
反应条件
copper(I) oxide; ammonia T=80°C; 16 h;
参考文献
Tetrahedron Letters, , vol. 42, # 19 p. 3251 - 3254
反应条件
1: 84 percent / aq. hydroxylammonium sulfate, aq. NaOH / 2 h / Ambient temperature 2: 69 percent Chromat. / acetyl chloride (AcCl) / 4 h / 100 - 130 °C 3: aq. NaOH / 1 h / 70 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 4 p. 887 - 891