Kolesnikow; Dawydowa
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2042,2044;engl.Ausg.S.2011
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Mazerolles; Lesbre
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1959 , vol. 248, p. 2018,2020
in tetrahydrofuran; diethyl ether
Soln. of CH2CHMgBr was added at -78°C to a suspd. AuBrSMe2 in Et2O followed by MeNC, mixt. was allowed to warm to -5°C;; Excess of Grignard was hydrolyzed at -5°C by NH4Cl soln., organic layer was sepd., dried, concd., cold pentane was added, crystals were obtained over 24 h; recrystd. at -78°C;;
参考文献
Puddephatt, Richard J.; Treurnicht, Ilse
Journal of Organometallic Chemistry, 1987 , vol. 319, p. 129 - 138
