5-三甲基甲硅烷基-2-糠酸合成路线 （共 10 条）
反应条件
1: furan-2-carboxylic acid With lithium diisopropyl amide in tetrahydrofuran; hexane T=-78°C; 2.5 h; 2: chloro-trimethyl-silane in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Dey, Tanmoy; Navarathne, Daminda; Invernale, Michael A.; Berghorn, Ian D.; Sotzing, Gregory A.
Tetrahedron Letters, 2010 , vol. 51, # 16 p. 2089 - 2091
反应条件
CO2 in not given (CH3)3Si(C4H2OLi) and solid CO2; hydrolysis;;
参考文献
Benkeser; Currie
Journal of the American Chemical Society, 1948 , vol. 70, p. 1780
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Gmelin Handbook: Si: MVol.C, 30, page 94 - 96
反应条件
n-butyllithium; diethyl ether anschliessend Behandeln mit festem Kohlendioxid;
参考文献
Gmelin Handbook: Si: MVol.C, 30, page 94 - 96
反应条件
water; silver(l) oxide in ethanol T=60°C;
参考文献
Lukevits, E.; Erchak, N. P.; Castro, I.; Popelis, Yu. Yu.; Kozyrev, A. K.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 9 p. 2062 - 2071,1830 - 1838
反应条件
sodium hydroxide; iodine
参考文献
Benkeser; Currie
Journal of the American Chemical Society, 1948 , vol. 70, p. 1780
Full Text View citing articles Show Details
Gmelin Handbook: Si: MVol.C, 30, page 94 - 96
反应条件
1: lithium di-isopropylamide (2 eqiv.) / hexane; tetrahydrofuran / 0.5 h / -78 °C 2: 0.40 g / tetrahydrofuran; hexane / -78 °C View Scheme
参考文献
Knight, David W.; Nott, Andrew P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1125 - 1131
反应条件
in tetrahydrofuran; hexane T=-78°C;
参考文献
Knight, David W.; Nott, Andrew P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1125 - 1131
反应条件
1: 1.) n-BuLi / 1.) THF, -78 deg C, 0.5 h, 2.) ether, -78 deg C to 25 deg C, 2 h 2: 97 percent / (nBu)4N(1+)*F(1-) / tetrahydrofuran / 12 h / 67 °C View Scheme
参考文献
Carpenter, Andrew J.; Chadwick, Derek J
Tetrahedron Letters, 1985 , vol. 26, # 14 p. 1777 - 1780
反应条件
Br2 in tetrachloromethane byproducts: 5-Brombrenzschleimsaeure; on boiling;;
参考文献
Benkeser; Currie
Journal of the American Chemical Society, 1948 , vol. 70, p. 1780
Full Text View citing articles Show Details
Gmelin Handbook: Si: MVol.C, 30, page 94 - 96
参考文献
Benkeser; Currie
Journal of the American Chemical Society, 1948 , vol. 70, p. 1780
