2-(三甲基硅氧基)丙烯合成路线 （共 98 条）
反应条件
zinc(II) chloride in dichloromethane T=22°C; 48 h;
参考文献
Reetz, Manfred T.; Maier, Wilhelm F.; Heimbach, Horst; Giannis, Athanassios; Anastassious, Georgia
Chemische Berichte, 1980 , vol. 113, # 12 p. 3734 - 3740
反应条件
zinc(II) chloride in dichloromethane T=22°C; 27 h; further reagents: TiCl4, SnCl4, ZrCl4, AlCl3;
参考文献
Reetz, Manfred T.; Maier, Wilhelm F.; Heimbach, Horst; Giannis, Athanassios; Anastassious, Georgia
Chemische Berichte, 1980 , vol. 113, # 12 p. 3734 - 3740
反应条件
para-toluenesulphonic acid silver salt in dichloromethane T=22°C; 15 h; ZnCl2;
参考文献
Reetz, Manfred T.; Maier, Wilhelm F.; Heimbach, Horst; Giannis, Athanassios; Anastassious, Georgia
Chemische Berichte, 1980 , vol. 113, # 12 p. 3734 - 3740
反应条件
titanium tetrachloride in dichloromethane T=-40°C; 4 h;
参考文献
Reetz, Manfred T.; Maier, Wilhelm F.; Heimbach, Horst; Giannis, Athanassios; Anastassious, Georgia
Chemische Berichte, 1980 , vol. 113, # 12 p. 3734 - 3740
反应条件
silver(l) oxide in dimethyl sulfoxide
参考文献
Ito,Y. et al.
Journal of the American Chemical Society, 1975 , vol. 97, p. 649 - 651
反应条件
pyridine; silver trifluoromethanesulfonate; trichloromethyl chloroformate 1) ether, 0 deg C, 15 min, 2) r.t., 2 h; Yield given. Multistep reaction;
参考文献
Takeda, Kazuyoshi; Ayabe, Akira; Kawashima, Hideki; Harigaya, Yoshihiro
Tetrahedron Letters, 1992 , vol. 33, # 7 p. 951 - 952
反应条件
dodecacarbonyltetrarhodium(0) in benzene T=100°C; 17 h;
参考文献
Sato, Susumu; Matsuda, Isamu; Izum, Yusuke
Tetrahedron Letters, 1987 , vol. 28, # 52 p. 6657 - 6660
Title/Abstract Full Text View citing articles Show Details
Sato, Susumu; Matsuda, Isamu; Izumi, Yusuke
Journal of Organometallic Chemistry, 1988 , vol. 352, p. 223 - 238
参考文献
Shimizu, Nobujiro; Miyahara, Toru; Mishima, Masaaki; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 6 p. 2032 - 2039
反应条件
trimethylsilyl trifluoromethanesulfonate; water; sodium hydrogencarbonate pentane, CH2Cl2, 78 deg C, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Smolyakova, I. P.; Smit, V. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 9.1. p. 1850 - 1853
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 9 p. 2036 - 2040
反应条件
trimethylsilyl trifluoromethanesulfonate; water; sodium hydrogencarbonate pentane, CH2Cl2, -78 deg C, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Smolyakova, I. P.; Smit, V. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 9.1. p. 1850 - 1853
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 9 p. 2036 - 2040
