hydrogenchloride; trichlorophosphate in N,N-dimethyl-formamide T=125°C;
参考文献
Shvekhgeimer, M.-G. A.; Kobrakov, K. I.; Sychev, S. S.; Promonenkov, V. K.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 4 p. 428 - 433
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 4 p. 514 - 519
New, James S.; Yevich, Joseph P.; Temple, Davis L.; New, Kimberly B.; Gross, Sharon M.; et al.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 3 p. 618 - 624
1: 3-Methylpyridine With fluorine in dichloromethane T=-78 - -50°C; 2: p-isocyanonitrobenzene in dichloromethane T=-50 - 0°C; 4 h; Further byproducts given. Title compound not separated from byproducts;
