反应条件
1: 1.) methyl lithium / 1.) ether, -78 deg C -> -40 deg C, 30 min, 2.) -78 deg C, 1 h, room temperature, 1 h
2: 1.) 5percent aq. sulfuric acid, 2.) 1N aq. sodium hydroxide / 1.) methanol, 5 min, 2.) ether, room temperature, 2 h
View Scheme
参考文献
Guittet, Eric; Julia, Sylvestre
Synthetic Communications, 1981 , vol. 11, # 9 p. 723 - 732
