2-苯基-1-苯并呋喃合成路线 (共 220 条)
反应条件
oxygen in N,N-dimethyl-formamide
T=135 - 140°C; 16 h;
参考文献
Swamy, Nalivela Kumara; Yazici, Arife; Pyne, Stephen G.
Journal of Organic Chemistry, 2010 , vol. 75, # 10 p. 3412 - 3419
反应条件
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4.17 h / 20 - 45 °C
2: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / N,N-dimethyl-formamide / 100 °C
View Scheme
参考文献
Chen, Wei; Zhang, Yicheng; Zhang, Lei; Wang, Min; Wang, Lei
Chemical Communications, 2011 , vol. 47, # 37 p. 10476 - 10478
反应条件
dichloro bis(acetonitrile) palladium(II); lithium carbonate in 1,4-dioxane
T=140°C; 40 h; Inert atmosphereSchlenk technique; Catalytic behavior;
参考文献
Loukotova, Lenka; Yuan, Kedong; Doucet, Henri
ChemCatChem, 2014 , vol. 6, # 5 p. 1303 - 1309
反应条件
1: 85 percent / KF/Al2O3 / 0.05 h / microwave irradiation (30 percent power)
2: 56 percent / PPh3; CuI; Pd / KF/Al2O3 / 0.06 h / microwave irradiation (100 percent power)
View Scheme
参考文献
Kabalka, George W.; Wang, Lei; Pagni, Richard M.
Tetrahedron, 2001 , vol. 57, # 38 p. 8017 - 8028
反应条件
1: 90 percent / KF/Al2O3 / 0.05 h / microwave irradiation (30 percent power)
2: 54 percent / PPh3; CuI; Pd / KF/Al2O3 / 0.06 h / microwave irradiation (100 percent power)
View Scheme
参考文献
Kabalka, George W.; Wang, Lei; Pagni, Richard M.
Tetrahedron, 2001 , vol. 57, # 38 p. 8017 - 8028
反应条件
1: 95 percent / BF3*OEt2 / acetic acid; toluene
2: 100 percent / imidazole / dimethylformamide
3: 69 percent
View Scheme
参考文献
Guthrie, Emma J.; MacRitchie, Jackie; Hartley, Richard C.
Tetrahedron Letters, 2000 , vol. 41, # 25 p. 4987 - 4990
反应条件
1: 100 percent / imidazole / dimethylformamide
2: 69 percent
View Scheme
参考文献
Guthrie, Emma J.; MacRitchie, Jackie; Hartley, Richard C.
Tetrahedron Letters, 2000 , vol. 41, # 25 p. 4987 - 4990
反应条件
dichloro bis(acetonitrile) palladium(II); potassium phosphate in 1,4-dioxane
T=140°C; 40 h; Inert atmosphereSchlenk technique;
参考文献
Loukotova, Lenka; Yuan, Kedong; Doucet, Henri
ChemCatChem, 2014 , vol. 6, # 5 p. 1303 - 1309
反应条件
hydrogen bromide; acetic acid
T=150°C;
参考文献
Stoermer; Frick
Chemische Berichte, 1924 , vol. 57, p. 27
反应条件
manganese triacetate in acetic acid
0.3 h; Heating;
参考文献
Oishi, Kazuki; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 1 p. 179 - 184