2-[(E)-2-羧基乙烯]苯甲酸合成路线 (共 32 条)
反应条件
1: polyphosphoric acid / 1.5 h / 110 °C 2: 90 percent / 2N HCl / 0.5 h / Heating View Scheme
参考文献
Narasimhan, N. S.; Kusurkar, S. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 4 p. 345 - 348
反应条件
formic acid; sodium hydroxide; palladium dichloride T=65°C; 24 h;
参考文献
Zhao, Jin; Dong, Hong-Bo; Yang, Ming-Yan; Du, Juan; Jiang, Jia-Zheng; Wang, Ming-An
Journal of Asian Natural Products Research, 2014 , vol. 16, # 3 p. 312 - 317
反应条件
trifluorormethanesulfonic acid T=25°C; 6 h;
参考文献
Rendy, Rendy; Zhang, Yun; McElrea, Aaron; Gomez, Alma; Klumpp, Douglas A.
Journal of Organic Chemistry, 2004 , vol. 69, # 7 p. 2340 - 2347
反应条件
Oxonereg; in water; acetonitrile
36 h; Reflux;
参考文献
Parida, Keshaba Nanda; Jhulki, Samik; Mandal, Susovan; Moorthy, Jarugu Narasimha
Tetrahedron, 2012 , vol. 68, # 47 p. 9763 - 9768,6
Title/Abstract Full Text Show Details
Parida, Keshaba Nanda; Jhulki, Samik; Mandal, Susovan; Moorthy, Jarugu Narasimha
Tetrahedron, 2012 , vol. 68, # 47 p. 9763 - 9768
反应条件
O,O'-dinitrodiphenyl diselenide; dihydrogen peroxide in tert-butyl alcohol
T=55°C; 6 h;
参考文献
Giurg, Miroslaw; Muchalski, Hubert; Kowal, Ewa
Synthetic Communications, 2012 , vol. 42, # 17 p. 2526 - 2539
反应条件
trimethyltin hydroxide in 1,2-dichloro-ethane
T=80°C; 9 h;
参考文献
Nicolaou; Estrada, Anthony A.; Zak, Mark; Lee, Sang Hyup; Safina, Brian S.
Angewandte Chemie - International Edition, 2005 , vol. 44, # 9 p. 1378 - 1382
反应条件
poly(bis-1,2-diphenylene) diselenide; dihydrogen peroxide in tetrahydrofuran; water
T=20°C; 20 h;
参考文献
Giurg; Syper; Mlochowski
Polish Journal of Chemistry, 2004 , vol. 78, # 2 p. 231 - 238
反应条件
2,2'-dinitro-4,4'-di(trifluoromethyl)diphenyl diselenide; dihydrogen peroxide in tert-butyl alcohol
T=55°C; 6 h;
参考文献
Giurg, Miroslaw; Muchalski, Hubert; Kowal, Ewa
Synthetic Communications, 2012 , vol. 42, # 17 p. 2526 - 2539
反应条件
palladium diacetate; potassium carbonate in water
T=100°C; 3 h;
参考文献
Bumagin, N. A.; More, P. G.; Beletskaya, I. P.
Journal of Organometallic Chemistry, 1989 , vol. 371, p. 397 - 402
反应条件
meta-chloroperoxybenzoic acid
参考文献
Fernholz
Chemische Berichte, 1951 , vol. 84, p. 110,118, 120