2,3-二甲基-6-溴喹噁啉合成路线 （共 7 条）
反应条件
0.0111111 h; Microwave irradiationNeat (no solvent);
参考文献
Morales-Castellanos, J. Jesus; Ramirez-Hernandez, Karina; Gomez-Flores, Nancy S.; Rodas-Suarez, Oscar R.; Peralta-Cruz, Javier
Molecules, 2012 , vol. 17, # 5 p. 5164 - 5176
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 1.5 h;
参考文献
Nakagawa, Masatoshi; Hanato, Hiroyuki; Tamura, Toshihiro
Patent: US2009/5557 A1, 2009 ;
Location in patent: Page/Page column 25-26 ;
反应条件
1: H2 / Raney nickel / ethanol View Scheme
参考文献
Dobrodei; El'tsov
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 620 - 629
反应条件
lithium in tetrahydrofuran T=-70 - -40°C; further lithium reagents: PhLi, BuLi; Product distribution;
参考文献
Dobrodei; El'tsov
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 620 - 629
反应条件
n-butyllithium 1.) THF, -50 deg C, 13 min, 2.) THF, -50 deg C, 2 h; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Dobrodei; El'tsov
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 620 - 629
反应条件
benzophenone; lithium 1.) THF, -50 deg C, 135 min, 2.) THF, room temp., overnight; Yield givenMultistep reaction;
参考文献
Dobrodei; El'tsov
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 620 - 629
反应条件
n-butyllithium
1.) THF, -50 deg C, 13 min, 2.) THF, -50 deg C, 2 h; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Dobrodei; El'tsov
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 620 - 629
