3,7-二甲基-1-辛烯-3-醇合成路线 （共 19 条）
反应条件
2-{2-(2-hydroxyethyl)thioethyl}thioethanol; hydrogen; Lindlar's catalyst T=30°C; P=1500.15 Torr; 8 h; Autoclave; Product distribution / selectivity;
参考文献
DSM IP ASSETS B.V.
Patent: US2012/53353 A1, 2012 ;
Location in patent: Page/Page column 5 ;
反应条件
1: 65 percent / H2 / 10percent Pd/C / methanol / 1 h / Ambient temperature 2: 65 percent / tetrahydrofuran / 3 h / Ambient temperature View Scheme
参考文献
Archiv der Pharmazie, , vol. 329, # 1 p. 27 - 34
反应条件
in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Fujishima, Toshie; Kagechika, Hiroyuki; Shudo, Koichi
Archiv der Pharmazie, 1996 , vol. 329, # 1 p. 27 - 34
反应条件
1: potassium hydroxide; ethanol; diethyl ether 2: palladium/calcium carbonate / Hydrogenation View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 28, p. 1458,1459
J. Gen. Chem. USSR (Engl. Transl.), , vol. 28, p. 1511,1512
反应条件
1: NaNH2 2: platinum; ethanol / Hydrogenation View Scheme
参考文献
Helvetica Chimica Acta, , vol. 23, p. 583
反应条件
1: aq. HCl / Heating 2: (i) Mg, THF, (ii) /BRN= 1731576/ View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 376 - 378
反应条件
(i) H2, Pd-BaSO4, (ii) /BRN= 3587269/; Multistep reaction;
参考文献
Acta Chemica Scandinavica, , vol. 29, # 10 B p. 1015 - 1023
反应条件
(i) Mg, THF, (ii) /BRN= 1731576/; Multistep reaction;
参考文献
Bulletin de la Societe Chimique de France, , p. 376 - 378
参考文献
Annales de Chimie (Cachan, France), , vol. <10>1, p. 364
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 174, p. 1551,1553
参考文献
Kuraray Co., Ltd.
Patent: US5955636 A1, 1999 ;
