4-(2-苯基乙炔)-苯胺合成路线 （共 28 条）
反应条件
nickel in N,N-dimethyl-formamide 0.25 h; Ambient temperature;
参考文献
Yasuhara; Kasano; Sakamoto
Journal of Organic Chemistry, 1999 , vol. 64, # 7 p. 2301 - 2303
反应条件
copper(l) iodide; potassium carbonate; triphenylphosphine in water T=100°C; 24 h; Inert atmosphere;
参考文献
Li, Tingyi; Sun, Peng; Yang, Hailong; Zhu, Yan; Yan, Hong; Lu, Linhua; Mao, Jincheng
Tetrahedron, 2012 , vol. 68, # 32 p. 6413 - 6419
反应条件
CuI(xantphos); caesium carbonate in N,N-dimethyl-formamide T=135°C; Sonogashira type reaction; 0.5 h; Inert atmosphereMicrowave irradiation;
参考文献
Tsai, Wen-Ting; Lin, Yun-Yung; Wang, Yu-Jen; Lee, Chin-Fa
Synthesis, 2012 , vol. 44, # 10 p. 1507 - 1510
反应条件
5 Au/Fe2O3; hydrogen in toluene T=60°C; P=15001.5 Torr; 1 h; Autoclave; chemoselective reaction;
参考文献
Organic Letters, , vol. 11, # 22 p. 5162 - 5165
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; water T=20°C; 12 h;
参考文献
Pena-Lopez, Miguel; Sarandeses, Luis A.; Perez Sestelo, Jose
European Journal of Organic Chemistry, 2013 , # 13 p. 2545 - 2554
反应条件
anhydrous iron chloride; potassium phosphate; triphenylphosphine in toluene T=135°C; Sonogashira coupling; 48 h; Inert atmosphere;
参考文献
Sawant, Dinesh N.; Tambade, Pawan J.; Wagh, Yogesh S.; Bhanage, Bhalchandra M.
Tetrahedron Letters, 2010 , vol. 51, # 20 p. 2758 - 2761
反应条件
KOC(O)Ph; triphenylphosphine; copper(l) chloride in 1,3-dimethyl-imidazolidin-2-one T=120°C; Sila-Sonogashira-Hagihara cross-coupling reaction; 12 h; Inert atmosphere;
参考文献
Ihara, Hideki; Ueda, Akinori; Suginome, Michinori
Chemistry Letters, 2011 , vol. 40, # 9 p. 972 - 974
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; ethanolamine in tetrahydrofuran T=60°C; Sonogashira coupling; 12 h;
参考文献
Mohamed Ahmed, Mohamed S.; Mori, Atsunori
Tetrahedron, 2004 , vol. 60, # 44 p. 9977 - 9982
反应条件
copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; (benzyl)-tri-(butyl)-ammonium chloride; sodium hydroxide; [(t-Bu)3PH]BF4 in water; toluene T=40°C; Sonogashira coupling; 22 h; Inert atmosphere;
参考文献
Bellina, Fabio; Lessi, Marco
Synlett, 2012 , vol. 23, # 5 p. 773 - 777
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 72 h / 20 °C 2: iron sulphate heptahydrate / methanol; water / 11 h / Reflux View Scheme
参考文献
Journal of the American Chemical Society, , vol. 131, # 32 p. 11458 - 11470
