4-(2-苯基乙炔)-苯胺合成路线 (共 28 条)
反应条件
1: CuCl2*2H2O / aq. HCl 2: KOH / dioxane 3: Sn, aq. HCl / ethanol View Scheme
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 33, # 1 p. 165 - 170,158 - 162
反应条件
1: Br2 2: KOH / methanol 3: Zn, aq. HCl View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 134 - 139
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 2043 - 2045
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 12 p. 2213 - 2215
反应条件
hydrogenchloride; sodium nitrite
1.) water, poly(ethylene glycol), CH2Cl2, 0 deg C; 2.) poly(ethylene glycol), CH2Cl2, from 0 deg C to RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Suzuki, Nobutaka; Azuma, Terukazu; Kaneko, Yoshihiro; Izawa, Yasuji; Tomioka, Hideo; Nomoto, Tateo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 645 - 648
反应条件
hydrogenchloride; sodium nitrite
multistep reaction; diazotization and Sandmeyer reaction in polyethylene glycol-CH2Cl2; 0 deg C to r.t.;
参考文献
Suzuki, Nobutaka; Kaneko, Yoshihiro; Nomoto, Tateo; Izawa, Yasuji
Journal of the Chemical Society, Chemical Communications, 1984 , # 22 p. 1523 - 1524
反应条件
hydrogenchloride; tin; sodium nitrite
1.) PEG-CH2Cl2, 0 deg C, 20 min, 2.) 0 to room temp., 3 h; Yield given. Multistep reaction;
参考文献
Suzuki, Nobutaka; Azuma, Terukazu; Watanabe, Koichi; Nomoto, Tateo; Izawa, Yasuji; Tomioka, Hideo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1951 - 1954
反应条件
hydrogenchloride; sodium nitrite
1.) water, poly(ethylene glycol), CH2Cl2, 0 deg C; 2.) poly(ethylene glycol), CH2Cl2, from 0 deg C to RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Suzuki, Nobutaka; Azuma, Terukazu; Kaneko, Yoshihiro; Izawa, Yasuji; Tomioka, Hideo; Nomoto, Tateo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 645 - 648
反应条件
hydrogenchloride; sodium nitrite
multistep reaction; diazotization and Sandmeyer reaction in polyethylene glycol-CH2Cl2; 0 deg C to r.t.;
参考文献
Suzuki, Nobutaka; Kaneko, Yoshihiro; Nomoto, Tateo; Izawa, Yasuji
Journal of the Chemical Society, Chemical Communications, 1984 , # 22 p. 1523 - 1524