1,4-双(苯乙炔基)苯合成路线 （共 41 条）
反应条件
triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) T=89°C; 0.05 h;
参考文献
Sanechika; Yamamoto; Yammoto
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 752 - 755
反应条件
tetra-n-butylammonium acetate; [5-Cl-2-{(4-Cl-phenyl)-[(E)-HO-imino]methyl}phenyl-PdCl]2 in 1-methyl-pyrrolidin-2-one T=110°C; Sonogashira coupling; 7.5 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 345, # 9-10 p. 1146 - 1158
反应条件
C28H61ClP2Pd2; diisopropylamine; zinc(II) chloride in tetrahydrofuran T=20°C; 2 h; Inert atmosphere;
参考文献
Finke, Aaron D.; Elleby, Eric C.; Boyd, Michael J.; Weissman, Haim; Moore, Jeffrey S.
Journal of Organic Chemistry, 2009 , vol. 74, # 22 p. 8897 - 8900
反应条件
sodium hydroxide; copper(l) iodide; tetra-(n-butyl)ammonium iodide; bis-triphenylphosphine-palladium(II) chloride in toluene T=80°C; Sonogashira coupling; 24 h;
参考文献
Chow; Wan; Low; Yeung
Journal of Organic Chemistry, 2001 , vol. 66, # 5 p. 1910 - 1913
反应条件
piperidine; triphenylphosphine; palladium dichloride in water; acetone T=60°C; Sonogashira reaction; 24 h;
参考文献
Shi, Shengyin; Zhang, Yuhong
Synlett, 2007 , # 12 p. 1843 - 1850
反应条件
copper(l) iodide; potassium carbonate; triphenylphosphine in dimethyl sulfoxide T=110°C; 24 h; Inert atmosphere;
参考文献
Qu, Xiaoming; Li, Tingyi; Sun, Peng; Zhu, Yan; Yang, Hailong; Mao, Jincheng
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 6938 - 6942
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=90°C; 3 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Jadhav, Deepak N.; Dasgupta, Priyabrata
Organic Letters, 2010 , vol. 12, # 9 p. 2048 - 2051
反应条件
tin(ll) chloride in ethanol; water; acetic acid T=60°C;
参考文献
Lydon, Donocadh P.; Porres, Laurent; Beeby, Andrew; Marder, Todd B.; Low, Paul J.
New Journal of Chemistry, 2005 , vol. 29, # 7 p. 972 - 976
反应条件
1: tri-phenyl-antimony With [bis(acetoxy)iodo]benzene in dichloromethane T=20°C; 7 h; 2: 1,4-bis(2-(trimethysilyl)ethynyl)-benzene With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; copper(l) iodide in acetonitrile T=50°C; 5 h; Further stages.;
参考文献
Kang, Suk-Ku; Ryu, Hyung-Chul; Hong, Young-Taek
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 7 p. 736 - 739
反应条件
[Pd(PPh3)2(OAc)2] in tetrahydrofuran T=66°C; 2 h;
参考文献
Sanechika; Yamamoto; Yammoto
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 752 - 755
