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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-苯乙烯基苯醇
合成路线
（共 36 条）
292638-84-7
+
533-58-4
2-碘苯酚
→
反应条件
18493-15-7
2-苯乙烯基苯醇
反应条件
Pd(NH3)2Cl2; tributyl-amine; tetrabutylammomium bromide in water Heck Reaction; 24 h; Reflux;
参考文献
Marti-Centelles, Rosa; Cejudo-Marin, Rocio; Falomir, Eva; Murga, Juan; Carda, Miguel; Alberto Marco
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 11 p. 3010 - 3015
292638-84-7
+
95-56-7
邻溴苯酚
→
反应条件
18493-15-7
2-苯乙烯基苯醇
反应条件
tetrabutylammomium bromide; potassium carbonate in water T=170°C; Heck Reaction; 0.166667 h; Microwave irradiationSealed tube;
参考文献
Marti-Centelles, Rosa; Cejudo-Marin, Rocio; Falomir, Eva; Murga, Juan; Carda, Miguel; Alberto Marco
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 11 p. 3010 - 3015
89-95-2
2-甲基苯甲醇
+
62673-31-8
苄基溴化锌
→
反应条件
18493-15-7
2-苯乙烯基苯醇
反应条件
chloro-trimethyl-silane; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; 8 h;
参考文献
Wang, Jin-Xian; Wang, Kehu; Zhao, Lianbiao; Li, Hongxia; Fu, Ying; Hu, Yulai
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 10-11 p. 1262 - 1270
271-89-6
氧茚
+
100-58-3
溴化苯基镁
→
反应条件
18493-15-7
2-苯乙烯基苯醇
反应条件
1: 2,3-benzofuran With [Ni0(1,5-cyclooctadiene)2]; C27H39N2(1+)*Cl(1-)*ClH; lithium chloride in tetrahydrofuran T=-30°C; 0.0333333 h; Inert atmosphere; 2: phenyl-magnesium bromide in tetrahydrofuran T=80°C; 16 h; Inert atmosphere; stereoselective reaction;
参考文献
Cornella, Josep; Martin, Ruben
Organic Letters, 2013 , vol. 15, # 24 p. 6298 - 6301
201230-82-2
+
92151-73-0
→
反应条件
955-10-2
3-苯基香豆素
+
73406-74-3
+
18493-15-7
2-苯乙烯基苯醇
反应条件
water; triethylamine; Rh6(CO)12 in 1,4-dioxane T=175°C; P=76000 Torr; 3 h;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 3 p. 477 - 483
90-02-8
水杨醛
+
100-51-6
苯甲醇
→
反应条件
18493-15-7
2-苯乙烯基苯醇
反应条件
1: benzyl alcohol With Et3P*HB r T=100°C; Wittig reaction; P=3750.38 - 5250.53 Torr; 8 h; Inert atmosphereNeat (no solvent); 2: With water; sodium hydroxide Wittig reaction; 0.0833333 h; Inert atmosphereSonication; 3: salicylaldehyde in water T=100°C; Wittig reaction; P=3750.38 - 5250.53 Torr; 0.5 h; Inert atmosphereMicrowave irradiation; optical yield given as percent dechemoselective reaction;
参考文献
McNulty, James; Das, Priyabrata; McLeod, David
Chemistry - A European Journal, 2010 , vol. 16, # 23 p. 6756 - 6760
92151-73-0
→
反应条件
955-10-2
3-苯基香豆素
+
73406-74-3
+
18493-15-7
2-苯乙烯基苯醇
反应条件
carbon monoxide; water; triethylamine; Rh6(CO)12 in 1,4-dioxane T=175°C; P=76000 Torr; 3 h; Yield given;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 3 p. 477 - 483
115032-32-1
→
反应条件
18493-15-7
2-苯乙烯基苯醇
反应条件
pyridinium p-toluenesulfonate in methanol Heating;
参考文献
Lion, Cedric J.; Matthews, Charles S.; Stevens, Malcolm F. G.; Westwell, Andrew D.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 4 p. 1292 - 1295
292638-84-7
+
936-02-7
水杨酰肼
→
反应条件
18493-15-7
2-苯乙烯基苯醇
反应条件
1: salicyloylhydrazine With copper(l) iodide; toluene-4-sulfonic acid; palladium dichloride in dimethyl sulfoxide; acetonitrile T=20°C; P=760.051 Torr; 1 h; 2: styrene in dimethyl sulfoxide; acetonitrile T=100°C; 3 h; stereoselective reaction;
参考文献
Zhang, Yong-Gang; Liu, Xiang-Lei; He, Zeng-Yang; Li, Xi-Ming; Kang, Hong-Jian; Tian, Shi-Kai
Chemistry - A European Journal, 2014 , vol. 20, # 10 p. 2765 - 2769
52805-92-2
1-甲氧基-2-(2-苯基乙烯基)苯
→
反应条件
18493-15-7
2-苯乙烯基苯醇
反应条件
boron tribromide in dichloromethane T=0 - 20°C;
参考文献
Ali; Kondo; Tsuda
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 5 p. 1130 - 1136
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