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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
18523-47-2
合成路线
（共 9 条）
18523-47-2
→
反应条件
14468-87-2
反应条件
oxalyl dichloride in dichloromethane T=20°C; 6 h;
参考文献
Vaidya, Aditya Sudheer; Karumudi, Bhargava; Mendonca, Emma; Madriaga, Antonett; Abdelkarim, Hazem; Van Breemen, Richard B.; Petukhov, Pavel A.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 15 p. 5025 - 5030
7719-09-7
氯化亚砜
+
18523-47-2
→
反应条件
14468-87-2
反应条件
12 h; Inert atmosphereReflux;
参考文献
Yu, Wei-Lun; Jones, Brian D.; Kang, Minjin; Hammons, Justin C.; La Clair, James J.; Burkart, Michael D.
Journal of Natural Products, 2013 , vol. 76, # 5 p. 817 - 823
18523-47-2
+
39145-59-0
苯-1,2-二胺盐酸盐
→
反应条件
5755-07-7
1,3,4,5-四氢-苯并[B][1,4]二氮杂革-2-酮
反应条件
1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide in N,N-dimethyl-formamide T=25°C; 0.0833333 h; 2: para-phenylenediamine hydrochloride in N,N-dimethyl-formamide T=25°C; 5 h; Inert atmosphereDarkness;
参考文献
Doebelin, Christelle; Schmitt, Martine; Antheaume, Cyril; Bourguignon, Jean-Jacques; Bihel, Frederic
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11335 - 11341
18523-47-2
+
591-19-5
间溴苯胺
→
反应条件
14088-96-1
1-(3-溴苯基)四氢-2H-咪唑-2-酮
反应条件
1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide in N,N-dimethyl-formamide T=25°C; 0.0833333 h; 2: 3-bromo-aniline in N,N-dimethyl-formamide T=50°C; 5 h; Inert atmosphereDarkness; TemperatureTime;
参考文献
Doebelin, Christelle; Schmitt, Martine; Antheaume, Cyril; Bourguignon, Jean-Jacques; Bihel, Frederic
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11335 - 11341
18523-47-2
+
59-88-1
盐酸苯肼
→
反应条件
16860-34-7
反应条件
1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide in N,N-dimethyl-formamide T=25°C; 0.0833333 h; 2: N-phenylhydrazine monohydrochloride in N,N-dimethyl-formamide T=25°C; 5 h; Inert atmosphereDarkness;
参考文献
Doebelin, Christelle; Schmitt, Martine; Antheaume, Cyril; Bourguignon, Jean-Jacques; Bihel, Frederic
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11335 - 11341
18523-47-2
+
74497-02-2
→
反应条件
1848-69-7
1-苯基咪唑啉-2-酮
反应条件
1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide in N,N-dimethyl-formamide T=25°C; 0.0833333 h; 2: aniline in N,N-dimethyl-formamide T=50°C; 5 h; Inert atmosphereDarkness; TemperatureTime;
参考文献
Doebelin, Christelle; Schmitt, Martine; Antheaume, Cyril; Bourguignon, Jean-Jacques; Bihel, Frederic
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11335 - 11341
18523-47-2
+
5345-54-0
3-氯-4-甲氧基苯胺
→
反应条件
88012-49-1
+
1099675-10-1
反应条件
1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide in N,N-dimethyl-formamide T=25°C; 0.0833333 h; 2: 1-amino-3-chloro-4-methoxybenzene in N,N-dimethyl-formamide T=50°C; 5 h; Inert atmosphereDarkness;
参考文献
Doebelin, Christelle; Schmitt, Martine; Antheaume, Cyril; Bourguignon, Jean-Jacques; Bihel, Frederic
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11335 - 11341
18523-47-2
+
19501-58-7
4-甲氧基苯肼盐酸盐
→
反应条件
6107-53-5
+
1471999-75-3
反应条件
1: 3-azidopropanoic acid With triethylamine; diisopropyl-carbodiimide in N,N-dimethyl-formamide T=25°C; 0.0833333 h; 2: 1-(4-methoxyphenyl)hydrazine hydrochloride in N,N-dimethyl-formamide T=25°C; 5 h; Inert atmosphereDarkness;
参考文献
Doebelin, Christelle; Schmitt, Martine; Antheaume, Cyril; Bourguignon, Jean-Jacques; Bihel, Frederic
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11335 - 11341
18523-47-2
+
693-13-0
N,N'-二异丙基碳二亚胺
→
反应条件
4128-37-4
对称二异丙基脲
反应条件
triethylamine in DMF-d7 T=25°C;
参考文献
Doebelin, Christelle; Schmitt, Martine; Antheaume, Cyril; Bourguignon, Jean-Jacques; Bihel, Frederic
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11335 - 11341
