R-1,1'-联-2-萘酚合成路线 （共 56 条）
反应条件
1: With copper(l) chloride; (+)-sparteine surrogate in methanol; dichloromethane T=-20 - 20°C; 24 h; Inert atmosphereDarkness; 2: With sodium hydrogencarbonate in methanol; dichloromethane; water T=-20°C; optical yield given as percent eeenantioselective reaction;
参考文献
Hu, Gang; Holmes, Daniel; Gendhar, Brina Fay; Wulff, William D.
Journal of the American Chemical Society, 2009 , vol. 131, # 40 p. 14355 - 14364
反应条件
1: in tetrahydrofuran T=-78 - -20°C; Inert atmosphere; 2: With water; ammonium chloride in tetrahydrofuran T=-20 - 20°C; Inert atmosphere; optical yield given as percent ee;
参考文献
Gaggero; Albanese
Tetrahedron, 2012 , vol. 68, # 35 p. 7129 - 7132
反应条件
1: in tetrahydrofuran T=-78 - -20°C; Inert atmosphere; 2: With water; ammonium chloride in tetrahydrofuran T=-20 - 20°C; Inert atmosphere; optical yield given as percent ee;
参考文献
Gaggero; Albanese
Tetrahedron, 2012 , vol. 68, # 35 p. 7129 - 7132
反应条件
1: in tetrahydrofuran T=-78 - -20°C; Inert atmosphere; 2: With water; ammonium chloride in tetrahydrofuran T=-20 - 20°C; Inert atmosphere; optical yield given as percent ee;
参考文献
Gaggero; Albanese
Tetrahedron, 2012 , vol. 68, # 35 p. 7129 - 7132
反应条件
1: in tetrahydrofuran T=-78 - -20°C; Inert atmosphere; 2: With water; ammonium chloride in tetrahydrofuran T=-20 - 20°C; Inert atmosphere; optical yield given as percent ee;
参考文献
Gaggero; Albanese
Tetrahedron, 2012 , vol. 68, # 35 p. 7129 - 7132
反应条件
oxygen; C26H28N2O9V2 in tetrachloromethane T=0°C; 168 - 192 h; Product distribution / selectivity;
参考文献
Chengdu Institute of Organic Chemistry Chinese Academy of Sciences
Patent: US2005/256345 A1, 2005 ;
Location in patent: Page/Page column 2-3; 5-6 ;
反应条件
1: With copper(l) chloride; (+)-sparteine surrogate in methanol; dichloromethane T=25°C; 24 h; Inert atmosphereDarkness; 2: With sodium hydrogencarbonate in methanol; dichloromethane; water optical yield given as percent eeenantioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 131, # 40 p. 14355 - 14364
反应条件
oxygen; oxovanadium(IV) in tetrachloromethane T=20°C; 144 h;
参考文献
Hon, Sang-Wen; Li, Chun-Hsin; Kuo, Jen-Huang; Barhate; Liu, Yi-Hung; Wang, Yu; Chen, Chien-Tien
Organic Letters, 2001 , vol. 3, # 6 p. 869 - 872
反应条件
in acetonitrile 3 h; Reflux;
参考文献
Tetrahedron: Asymmetry, , vol. 23, # 18-19 p. 1327 - 1331,5
反应条件
Arthrobacter sp. lipase in aq. phosphate buffer; dimethyl sulfoxide T=25°C; pH=7; 44 h; Resolution of racemateEnzymatic reaction; SolventConcentration; enantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 101, p. 35 - 39
