R-1,1'-联-2-萘酚合成路线 （共 56 条）
反应条件
Arthrobacter sp. lipase in aq. phosphate buffer; N,N-dimethyl-formamide T=25°C; pH=7; 24 h; Resolution of racemateEnzymatic reaction; Solvent; enantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 101, p. 35 - 39
反应条件
(8S,9R)-(-)-N-benzyl-cinchonidinium chloride in acetonitrile resolution of racemate; 4 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 65, # 20 p. 6319 - 6337
反应条件
1: in tetrahydrofuran T=-78 - -20°C; Inert atmosphere; 2: With water; ammonium chloride in tetrahydrofuran T=-20 - 20°C; Inert atmosphere; optical yield given as percent ee;
参考文献
Tetrahedron, , vol. 68, # 35 p. 7129 - 7132
反应条件
boron tribromide in dichloromethane T=-78°C;
参考文献
Journal of the American Chemical Society, , vol. 104, # 3 p. 879 - 881
反应条件
1: water / cholesterol esterase, sodium taurocholate / diethyl ether / 65 h / pH = 7.2 2: CH3ONa / methanol / 2 h / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 13 p. 4953 - 4959
反应条件
water; cholesterol esterase in diethyl ether T=25°C; catalyst activated by sodium taurocholate; pH = 7.00; rate of hydrolysis (relative to cholesterol acetate); Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 111, # 13 p. 4953 - 4959
反应条件
water; cholesterol esterase in diethyl ether T=25°C; catalyst activated by sodium taurocholate; pH = 7.00; rate of hydrolysis (relative to cholesterol acetate); Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 111, # 13 p. 4953 - 4959
反应条件
water; cholesterol esterase in diethyl ether T=25°C; catalyst activated by sodium taurocholate; pH = 7.00; rate of hydrolysis (relative to cholesterol acetate); Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 111, # 13 p. 4953 - 4959
反应条件
water; cholesterol esterase in diethyl ether T=25°C; catalyst activated by sodium taurocholate; pH = 7.00; rate of hydrolysis (relative to cholesterol acetate); Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 111, # 13 p. 4953 - 4959
反应条件
1: Jones reagent 2: MCPBA, NaHCO3 / CH2Cl2 / 21 h / Heating 3: 17percent KOH / methanol 4: boron tribromide / CH2Cl2 / -78 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 3 p. 879 - 881
