R-1,1'-联-2-萘酚合成路线 （共 56 条）
反应条件
1: MCPBA, NaHCO3 / CH2Cl2 / 21 h / Heating 2: 17percent KOH / methanol 3: boron tribromide / CH2Cl2 / -78 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 3 p. 879 - 881
反应条件
1: 17percent KOH / methanol 2: boron tribromide / CH2Cl2 / -78 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 3 p. 879 - 881
反应条件
water; cholesterol esterase in diethyl ether T=25°C; catalyst activated by sodium taurocholate; pH = 7.00; rate of hydrolysis (relative to cholesterol acetate); Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 111, # 13 p. 4953 - 4959
反应条件
water; cholesterol esterase in diethyl ether T=25°C; catalyst activated by sodium taurocholate; pH = 7.00; rate of hydrolysis (relative to cholesterol acetate); Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 111, # 13 p. 4953 - 4959
反应条件
water; cholesterol esterase in diethyl ether T=25°C; catalyst activated by sodium taurocholate; pH = 7.00; rate of hydrolysis (relative to cholesterol acetate); Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 111, # 13 p. 4953 - 4959
反应条件
potassium hydroxide in ethanol
参考文献
Bulletin of the Chemical Society of Japan, , vol. 57, # 7 p. 1943 - 1947
反应条件
Candida antarctica lipase B; acetophenone; butan-1-ol in various solvent(s) T=60°C; 96 h;
参考文献
Aoyagi, Naoto; Ogawa, Naomi; Izumi, Taeko
Tetrahedron Letters, 2006 , vol. 47, # 28 p. 4797 - 4801
反应条件
1: 95 percent / O2 / chiral V2O9C26H28N2 / CCl4 / 0 °C 2: NaH / tetrahydrofuran / 5 h / 0 - 20 °C 3: 3.8 g / K2CO3; Pd(PPh3)4 / methanol / 5 h / Heating 4: 87 percent / Et3N / CH2Cl2 / 2 h / 0 - 20 °C 5: Pd(PPh3)4; HCO2H; i-Pr2NEt / dimethylformamide / 80 °C 6: aq. HCl / CHCl3; ethanol / 2 h / 65 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 20 p. 7921 - 7924
反应条件
Pseudomonas sp. lipoprotein lipase in isopropyl alcohol; acetone T=40°C; 120 h;
参考文献
Juarez-Hernandez, Marcela; Johnson, Dean V.; Holland, Herbert L.; McNulty, James; Capretta, Alfredo
Tetrahedron Asymmetry, 2003 , vol. 14, # 3 p. 289 - 291
反应条件
1: in methanol T=50°C; 1 h; 2: With hydrogenchloride in water; ethyl acetate Product distribution / selectivity;
参考文献
WO2011/86566 A1, ;
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